Synthesis
Mixture | Acid leaching of carletonite |
SDA | H+ |
Temperature | 0.01 °C |
Duration | 3 d |
Conditions | static |
Reference |
Marler & Grosskreuz (2024): Crystals(MDPI), Volume 14, Issue , Pages No. 326. |
Crystal Structure
Structurally nearly identical materials | None |
Crystal chemically related materials | None |
Chemical composition per unit cell | H32Si64O144 |
Lattice parameters of the 2D cell of the layer |
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Lattice parameters related to the stacking direction |
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Space group | I4/mcm |
XRD reflections representing the 2D cell of the layer |
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XRD reflections representing the layer-layer distance |
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Reference |
Marler & Grosskreuz (2024): Crystals(MDPI), Volume 14, Issue , Pages No. 326. |
Properties
Density (calculated) | 1.736 g/cm3 |
Condensation product | amorphous |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
0 | 0 | 2 | 2 | 8.633 | 4.6 | 10.234 |
1 | 1 | 0 | 4 | 8.993 | 10.2 | 9.826 |
1 | 1 | 2 | 8 | 12.478 | 0.9 | 7.088 |
2 | 0 | 0 | 4 | 12.731 | 100.0 | 6.948 |
2 | 1 | 1 | 16 | 14.886 | 11.2 | 5.946 |
2 | 0 | 2 | 8 | 15.402 | 0.9 | 5.748 |
0 | 0 | 4 | 2 | 17.316 | 50.6 | 5.117 |
2 | 2 | 0 | 4 | 18.041 | 48.5 | 4.913 |
2 | 1 | 3 | 16 | 19.304 | 47.6 | 4.594 |
1 | 1 | 4 | 8 | 19.544 | 0.1 | 4.538 |
2 | 2 | 2 | 8 | 20.032 | 0.6 | 4.429 |
3 | 1 | 0 | 8 | 20.192 | 7.2 | 4.394 |
2 | 0 | 4 | 8 | 21.551 | 13.1 | 4.120 |
3 | 1 | 2 | 16 | 21.996 | 0.8 | 4.038 |
3 | 2 | 1 | 16 | 23.469 | 1.7 | 3.787 |
. | . | . | . | . | . | |
2 | 2 | 4 | 8 | 25.108 | 2.6 | 3.544 |
4 | 0 | 0 | 4 | 25.622 | 0.0 | 3.474 |
2 | 1 | 5 | 16 | 26.045 | 8.3 | 3.419 |
0 | 0 | 6 | 2 | 26.101 | 5.0 | 3.411 |
3 | 2 | 3 | 16 | 26.542 | 25.6 | 3.356 |
3 | 1 | 4 | 16 | 26.720 | 0.1 | 3.334 |
4 | 1 | 1 | 16 | 26.787 | 0.7 | 3.325 |
4 | 0 | 2 | 8 | 27.084 | 0.3 | 3.290 |
3 | 3 | 0 | 4 | 27.205 | 0.2 | 3.275 |
1 | 1 | 6 | 8 | 27.659 | 0.1 | 3.223 |
3 | 3 | 2 | 8 | 28.592 | 0.0 | 3.119 |
4 | 2 | 0 | 8 | 28.707 | 44.9 | 3.107 |
2 | 0 | 6 | 8 | 29.140 | 0.4 | 3.062 |
4 | 1 | 3 | 16 | 29.538 | 8.2 | 3.022 |
4 | 2 | 2 | 16 | 30.031 | 0.5 | 2.973 |
4 | 0 | 4 | 8 | 31.091 | 0.2 | 2.874 |
3 | 2 | 5 | 16 | 31.866 | 3.0 | 2.806 |
2 | 2 | 6 | 8 | 31.913 | 2.3 | 2.802 |
3 | 3 | 4 | 8 | 32.429 | 0.2 | 2.759 |
4 | 3 | 1 | 16 | 32.486 | 0.9 | 2.754 |
5 | 1 | 0 | 8 | 32.837 | 0.7 | 2.725 |
3 | 1 | 6 | 16 | 33.221 | 0.3 | 2.695 |
4 | 2 | 4 | 16 | 33.720 | 6.6 | 2.656 |
2 | 1 | 7 | 16 | 33.854 | 13.4 | 2.646 |
5 | 1 | 2 | 16 | 34.016 | 0.3 | 2.633 |
4 | 1 | 5 | 16 | 34.442 | 0.5 | 2.602 |
4 | 3 | 3 | 16 | 34.829 | 0.2 | 2.574 |
5 | 2 | 1 | 16 | 35.021 | 0.2 | 2.560 |
0 | 0 | 8 | 2 | 35.045 | 2.2 | 2.558 |
1 | 1 | 8 | 8 | 36.253 | 0.2 | 2.476 |
4 | 4 | 0 | 4 | 36.550 | 1.6 | 2.456 |
4 | 0 | 6 | 8 | 36.900 | 0.0 | 2.434 |
Atom | x | y | z | Biso | Occ. | |
---|---|---|---|---|---|---|
Si1 | 0.0957 | 0.2462 | 0.4223 | 0.67 | 1.000 | |
Si2 | 0.2341 | 0.1038 | 0.3520 | 0.67 | 1.000 | |
O1 | 0.1483 | 0.1557 | 0.3913 | 0.86 | 1.000 | |
O2 | 0.2530 | 0.0092 | 0.3937 | 0.86 | 1.000 | |
O3 | 0.2076 | 0.0849 | 0.2740 | 0.86 | 1.000 | |
O4 | 0.1650 | 0.6650 | 0.3554 | 0.86 | 1.000 | |
O5 | 0.1597 | 0.6597 | 0.0964 | 0.86 | 1.000 | |
O6 | 0.0857 | 0.2265 | 0.5000 | 0.86 | 1.000 |
User Cell Range (natural numbers 1-5):