References

[1] Y. Ide, N. Kagawa, M.Sadakane, T. Sano: Precisely designed layered silicate as an effective and highly selective CO2 adsorbent. Chem. Commun. 49, 9027-9029, 2013.

[2] S. Toriya, S. Kobayashi, T. Takei, M. Fuji, T. Watanabe, M.Chikazawa: Modification of interlayer space of kanemite with trimethylsilyl groups: structure and adsorption properties. Colloid Polym. Sci. 281, 1121–1126, 2003.

[3] e.g. F. Kooli, F. Mizukami, Y. Kiyozumi, Y. Akiyama: Hydrothermal conversion of Na-magadiite to a new silicate layered structure in a TMAOH-water-1,4-dioxane system. J. Mater. Chem. 11, 1946-1950, 2001.

[4] K. Kuroda: Silica-Based Mesoporous Molecular Sieves Derived from a Layered Polysilicate Kanemite - A Review. J. Porous Materials 3, 107-114, 1996.

[5] S. Shimizu, Y. Kiyozumi, K. Maeda, F. Mizukami, G. PalBorbely, R.M. Mihalyi, H.K. Beyer: Transformation of intercalated layered silicates to zeolites in the solid state. Adv. Mater. 8, 759–762, 1996.

[6] H. Gies, U. Müller, B. Yilmaz, T. Tatsumi, B. Xie, F. S. Xiao, X. H. Bao, W. P. Zhang and D. de Vos, Interlayer expansion of the layered zeolite precursor RUB-39: a universal method to synthesize functionalized microporous silicates. Chem. Mater. 23, 2545-2554, 2011.

[7] S. Inagaki, Y. Sakamoto, Y. Fukushima and O. Terasaki, Chem. Mater. 8, 2089, 1996.

[8] J.F. Ruan, P. Wu, B. Slater, Z.L. Zhao, L.L. Wu, O. Terasaki: Structural characterization of inter-layer expanded zeolite prepared from ferrierite lamellar precursor. Chem. Mater. 21, 2904–2911, 2009.

[9] K.W. Park, J.H. Jung, S.K. Kim, O.Y. Kwon: Interlamellar silylation of magadiite by octyl triethoxysilane in the presence of dodecylamine. Appl. Clay Sci. 46, 251–254, 2009.

[10] A. Corma, V. Fornes, J. Martinez-Triguero and S.B. Pergher: Delaminated zeolites: Combining the benefits of zeolites and mesoporous materials for catalytic uses. J. Catal. 186, 57-63,1999,

[11] A. Corma, U. Diaz, M. E. Domine, V. Fornes, New aluminosilicate and titanosilicate delaminated materials active for acid catalysis, and oxidation reactions using H2O2. J. Am. Chem. Soc. 122, 2804-2809, 2000,

[12] A. Corma, V. Fornes, U. Diaz: ITQ-18 a new delaminated stable zeolite. Chem. Commun. 2001, 2642-2643, 2001.

[13] A. Corma, U. Diaz, M. E. Domine, V. Fornes: AlITQ-6 and TiITQ-6: Synthesis, characterization, and catalytic activity. Angew. Chem. Int. Ed. 39, 1499-1501, 2000

[14] M.E. Leonowicz, J.A. Lawton, S.L. Lawton, M.K. Rubin: MCM-22 - A Molecular-Sieve with 2 Independent Multidimensional Channel Systems. Science 264, 1910-1930,1994.

[15] L. Schreyeck, P. Caullet, J. C. Mougenel, J. L. Guth and B. Marler: PREFER: a new layered (alumino) silicate precursor of FER-type zeolite. Microporous Mater. 6, 259-271,1996,

[16] B. Marler and H. Gies: Hydrous layer silicates as precursors for zeolites obtained through topotactic condensation. Eur. J. Mineral 24, 405-428, 2012.

[17] W. Schwieger and G. Lagaly: Alkali silicates and crystalline silicic acids, in “Handbook of Layered Materials” (S. M. Auerbach, K. A. Carrado, P. K. Dutta, eds.) Marcel Dekker, New York, 541-629, 2004.

[18] F.S.O. Ramos, M.K. de Pietre, H.O. Pastore: Lamellar zeolites: an oxymoron? RSC Advances, A review 3, 2084-2111, 2013.

[19] C. Baerlocher, L.B. McCusker, D.H. Olson, (2007): a) Atlas of Zeolite Framework Types, Sixth Revised Edition, Elsevier, Amsterdam. b) Database of Zeolite Structures: http://www.iza-structure.org/databases/

[20] M.M.J. Treacy, J.B. Higgins: Collection of simulated powder patterns for zeolites, Fifth Revised Edition, Elsevier, Amsterdam (2007).

[21] G. Lagaly, K. Beneke, A. Weiss: Crystalline Silicic Acid H2Si14O29 * 5 H2O with Layer Structure and Capability of Formation of Intercalation Compounds. Z. Naturforsch. B 28, 234-238, 1973.

[22] G. Lagaly, K. Beneke, H. Kammermeier (1979): New Modifications of Silica, Z. Naturforsch. Section B 34b, 666-674.

[23] B.M. Micjuk, L.L. Gorogoe´kaja, A.L. Rastrenenka: Geochimija 1976, 803–814, 1976.

[24] K. Beneke, G. Lagaly: Kenyaite-synthesis and properties. Am. Miner. 68, 818-826, 1983.

[25] G. Lagaly, R. Matouschek: Crystalline Silicic Acids from Apophyllite, Carletonite, Gillespite. N. Jb. Miner. Abh. 138, 81-93, 1980.

[26] A. Pabst: The Structure of leached Gillespite. Am. Miner. 43, 970-980, 1958.

[27] K. Beneke, H.H. Kruse, G. Lagaly: Crystalline Silicic Acid with distinct intracrystalline reactivity. Z. anorg. allg. Chem. 518, 65-76, 1984.

[28] A.J. Gude, and A. Schepard: Silhydrite, 3SiO2*H2O, A new mineral from Trinity County, California, Am. Miner. 57, 1053-1065, 1972.

[29] A.A. Colville, C.P. Anderson, P.M. Black: Refinement of the Crystal Structure of Apophyllite: I. X-ray diffraction and physical properties , Am. Miner. 56, 1222-1233, 1971.

[30] N. Tsunoji, M. Fukuda, K. Yoshida, Y. Sasaki, T. Ikeda, Y. Ide, M. Sadakane, T. Sano: Characterization of layered silicate HUS-5 and formation of novel nanoporous silica through transformation of HUS-5 ion-exchanged with alkylammonium cations, J. Mater. Chem. A 1, 9680-9688, 2013.

[31] G.Y. Chao: Crystal-Structure of Carletonite - KNa4Ca4Si8O18(CO3)4(F,OH) H2O - Double-Sheet Silicate. Am. Miner. 57, 765-778, 1972.

[32] W. J. Roth, C.T. Kresge: Intercalation chemistry of NU-6(1), the layered precursor to zeolite NSI, leading to the pillared zeolite MCM-39(Si). Microporous Mesoporous Mater. 144, 158-161, 2011.

[33] L.D. Rollmann, J.L. Schlenker, J.L., Lawton L., Kennedy C.L., Kennedy G.J. MCM-69, a novel layered analogue of EU-19, Microporous Mesoporous Mater. 53, 179-193, 2002.

[34] C. L. Kennedy, G. J. Kennedy, S. L. Lawton, L. D. Rollmann, J. L. Schlenker: Synthetic crystalline MCM-69, its synthesis and use. US Patent 6419891 B1.

[35] T. Ikeda, Y. Akiyama, Y. Oumi, A. Kawai, F. Mizukami : The topotactic conversion of a novel layered silicate into a new framework zeolite. Angew. Chem. Intern. Ed. 43, 4892-4896 (2004).

[36] F. Kooli Y. Kiyozumi V. Rives, F. Mizukami: Synthesis and textural characterization of a new microporous silica material. Langmuir 18, 4103-4110, 2002.

[37] N. Tsunoji, T. Ikeda, Y. Ide, M. Sadakane, T. Sano: Synthesis and characteristics of novel layered silicates HUS-2 andHUS-3 derived from a SiO2-choline hydroxide-NaOH-H2O system, J. Mater. Chem. 22, 13682-13690, 2012.

[38] L.M. Knight, M.A. Miller, S.C. Koster, M.G. Gatter, A.I. Benin, R.R. Willis, G.J. Lewis, R.W. Broach: UZM-13, UZM-17, UZM-19 and UZM-25: Synthesis and structure of new layered precursors and a zeolite discovered via combinatorial chemistry techniques. in ” Studies in Surface Science and Catalysis”, R. Xu, Z. Gao, J. Chen, W. Yan, eds., Elsevier, Amsterdam, 170A, 338-346, 2007.

[39] T. Ikeda, S. Kayamori, F. Mizukami: Synthesis and crystal structure of layered silicate PLS-3 and PLS-4 as a topotactic zeolite precursor. J. Mater. Chem. 19, 5518–5525, 2009.

[40] D.L. Dorset and G.J. Kennedy: Crystal structure of MCM-65: an alternative linkage of ferrierite layers. J. Phys. Chem. B 108, 15216-15222, 2004.

[41] J.E. Schmidt, D. Xie, M.E. Davis: High-silica, heulandite-type zeolites prepared by direct synthesis and topotactic condensation. J. Mater. Chem. A 3, 12890-12897, 2015.

[42] B. Marler, Z. Li, G. Wang, H. Gies: Synthesis and structure of two new layered silicate hydrates, RUB-52 and RUB-53. Acta Cryst. A 67, C650 (2011).

[43] A. Carati, C. Rizzo, R. Millini, E. Di Paola, E. Montanari, S. Zanardi: Synthesis of zeolites using N,N′-tetramethylen-bis-(N-methylpiperidinium) dyhydroxide as directing agent. Proc. of the 4th Int. FEZA Conference (eds: A. Gedeon, P. Massiani, F. Babonneau) 269-272, 2008.

[44] R. Millini, G. Perego, W.O. Parker, G. Belussi, L. Carluccio: Layered structure of ERB-1 microporous borosilicate precursor and its intercalation properties towards polar molecules, Microporous Mater. 4, 221-230, 1995.

[45] a) Camblor, M.A., Corma, A., Diaz-Cabanas, M.-J., Baerlocher, C. (1998): Synthesis and structural characterization of MWW type zeolite ITQ-1, the pure silica analog of MCM-22 and SSZ-25, J. Phys. Chem. B, 102, 44-51, b) Camblor, M.A., Corell, C., Corma, A., Diaz-Cabanas, M.-J., Nicolopoulos, S., Gonzalez-Calbet, J.M. and Vallet-Regi, M. (1996): A new microporous polymorph of silica isomorphous to zeolite MCM-22. Chem. Mater., 8, 2415-2417.

[46] L. Puppe and J. Weisser: Crystalline alumosilicate PSH-3 and its process of preparation. US Patent 4 439 409, 1984.

[47] S.I. Zones: New Zeolite SSZ-25, Eur. Patent EP 0231860 A2, 1987.

[48] A.S. Fung, S.L. Lawton, W.J. Roth: Synthetic layered MCM-56, its synthesis and use. U.S. patent 5,362,697, 1994.

[49] W.J.Roth, D.L. Dorset, G.J. Kennedy: Discovery of new MWW family zeolite EMM-10: Identification of EMM-10P as the missing MWW precursor with disordered layers. Microporous Mesoporous Mater. 142, 168-177, 2011.

[50] Brenn, U., Ernst, H., Freude, D., Herrmann, R., Jahnig, R., Karge, H.G., Karger, J., Konig, T., Madler, B., Pingel, U.T., Prochnow, D., Schwieger, W. (2000): Synthesis and characterization of the layered sodium silicate Ilerite, Microporous Mesoporous Mater. 40, 43-52.

[51] R.K Iler: Ion exchange properties of a crystalline hydrated silica, J. Colloid Science 19, 648-657, 1964.

[52] Massueger, L., Baerlocher, C., McCusker, L.B., Zwijnenburg, M.A. (2007): Synthesis and structure analysis of the layer silicate DLM-2, Microporous Mesoporous Mater. 105, 75-81

[53] J. Plevert, T. Plevert, T. Tatsumi: Silicon vacancy ordering in pure silica TMA-Nu-1: opening the pores of a clathrasil, Abstract for the International Symposium on Zeolites and MicroPorous Crystals, P-026, Hiroshima, Japan 2012.

[54] A. Bhaumik and T. Tatsumi: Pure silica NU-1 and Na- and Al-free Ti-NU-1 synthesized by the dry gel conversion method, Microporous Mesoporous Mater. 34, 1-7, 2000.

[55] K. Beneke and G. Lagaly: Kanemite - innercrystalline reactivity and relations to other sodium silicates. Am. Miner. 62, 763-771, 1977

[56] A.J. Blake, K.R. Franklin, B.M. Lowe: Preparation and properties of piperazine silicate (EU-19) and a silica polymorph (EU-20). J. Chem. Soc. Dalton Trans. 1988, 2513-2517, 1988

[57] B. Marler, M.A. Camblor, H. Gies: The disordered structure of silica zeolite EU-20b, obtained by topotactic condensation of the piperazinium containing layer silicate EU-19, Microporous Mesoporous Mater. 90, 87-101, 2006.

[58] M. E. Leonowicz, J. A. Lawton, S. L. Lawton, M. K. Rubin: MCM-22: A Molecular Sieve with Two Independent Multidimensional Channel Systems. Science 264, 1910-1913, 1994.

[59] Condensation of disilicic acid to cristobalite

[91] A. Corma, V.Fornes, J.M. Guil, S. Pergher, T.M.L. Maesen, J.G. Buglass: Preparation, characterisation and catalytic activity of ITQ-2, a delaminated zeolite. Microporous Mesoporous Mater. 38, 301-309, 2000.

[92] A. Corma, U. Diaz, M.E. Domine, V. Fornes: New Aluminosilicate and Titanosilicate Delaminated Materials Active for Acid Catalysis, and Oxidation Reactions Using H2O2. J. Am. Chem. Soc. 122, 2804–2809, 2000.

[93] H. Gies, U. Müller, B. Yilmaz, M. Feyen, T. Tatsumi, H. Imai, H. Y. Zhang, B. Xie, F. S. Xiao, X. H. Bao, W. P. Zhang, T. De Baerdemaeker, D. De Vos: Interlayer Expansion of the Hydrous Layer Silicate RUB-36 to a Functionalized, Microporous Framework Silicate: Crystal Structure Analysis and Physical and Chemical Characterization. Chem. Mater. 24, 1536-1545, 2012.

[94], P. Chlubná, W.J. Roth, A. Zukal, M. Kubů, J. Pavlatová: Pillared MWW zeolites MCM-36 prepared by swelling MCM-22P in concentrated surfactant solutions, Catalysis Today 179, 35– 42, 2012.

[95] A. Corma, U. Díaz, T. Garcıá, G. Sastre, A. Velty: Multifunctional Hybrid Organic-Inorganic Catalytic Materials with a Hierarchical System of Well-Defined Micro- and Mesopores, J. Am. Chem. Soc. 132, 15011–15021, 2010.

[96] M. Choi, K. Na, J. Kim, Y. Sakamoto, O. Terasaki, R. Ryoo: Stable single-unit-cell nanosheets of zeolite MFI as active and long-lived catalysts, Nature 461, 246-250, 2009

[97] W.J. Roth, P. Nachtigall, R.E. Morris, J. Cejka: Two-Dimensional Zeolites: Current Status and Perspectives, Chem. Reviews 114, 4807-4837, 2014 .