Synthesis
Mixture | SiO2 : SDA: H2O |
SDA | N,N,N-Trimethyl-1-Adamantammonium hydroxide |
Temperature | 150.00 °C |
Duration | 17 d |
Conditions | rotated (60 rpm) |
Reference |
Rubin & Chu (1990): U.S. Patent, Volume 4, Issue Nr. 4,954,325, Pages . |
Crystal Structure
Comment | Unit cell parameters and indices are based on an idealized hexagonal symmetry |
Structurally nearly identical materials | |
Crystal chemically related materials | None |
Chemical composition per unit cell | Na(C5H12N)9 [B6Si66O147] ∙ 20 H2O |
Lattice parameters of the 2D cell of the layer |
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Lattice parameters related to the stacking direction |
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Space group | unk. |
XRD reflections representing the 2D cell of the layer |
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XRD reflections representing the layer-layer distance |
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Reference |
(): , Volume , Issue , Pages . |
Properties
Density (calculated) | 1.935 g/cm3 |
Condensation product | MCM-22 (zeolite framework type: MWW) [58] |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
0 | 0 | 1 | 2 | 3.285 | 88.0 | 26.874 |
0 | 0 | 2 | 2 | 6.573 | 88.4 | 13.437 |
1 | 0 | 0 | 6 | 7.172 | 58.9 | 12.315 |
1 | 0 | 1 | 12 | 7.891 | 50.9 | 11.196 |
1 | 0 | 2 | 12 | 9.734 | 73.4 | 9.079 |
0 | 0 | 3 | 2 | 9.866 | 0.0 | 8.958 |
1 | 0 | 3 | 12 | 12.208 | 2.4 | 7.244 |
1 | 1 | 0 | 6 | 12.439 | 0.0 | 7.110 |
1 | 1 | 1 | 12 | 12.869 | 11.3 | 6.874 |
0 | 0 | 4 | 2 | 13.167 | 14.5 | 6.718 |
1 | 1 | 2 | 12 | 14.081 | 2.2 | 6.285 |
2 | 0 | 0 | 6 | 14.373 | 1.3 | 6.158 |
2 | 0 | 1 | 12 | 14.747 | 10.9 | 6.002 |
1 | 0 | 4 | 12 | 15.009 | 7.7 | 5.898 |
2 | 0 | 2 | 12 | 15.819 | 0.9 | 5.598 |
. | . | . | . | . | . | |
1 | 1 | 3 | 12 | 15.901 | 13.2 | 5.569 |
0 | 0 | 5 | 2 | 16.480 | 5.1 | 5.375 |
2 | 0 | 3 | 12 | 17.463 | 1.2 | 5.074 |
1 | 0 | 5 | 12 | 17.993 | 5.5 | 4.926 |
1 | 1 | 4 | 12 | 18.152 | 3.8 | 4.883 |
2 | 1 | 0 | 12 | 19.051 | 1.5 | 4.655 |
2 | 1 | 1 | 24 | 19.338 | 0.0 | 4.586 |
2 | 0 | 4 | 12 | 19.540 | 32.9 | 4.539 |
0 | 0 | 6 | 2 | 19.806 | 62.9 | 4.479 |
2 | 1 | 2 | 24 | 20.173 | 2.2 | 4.398 |
1 | 1 | 5 | 12 | 20.700 | 20.4 | 4.288 |
1 | 0 | 6 | 12 | 21.090 | 0.4 | 4.209 |
2 | 1 | 3 | 24 | 21.497 | 0.0 | 4.130 |
3 | 0 | 0 | 6 | 21.631 | 0.0 | 4.105 |
3 | 0 | 1 | 12 | 21.885 | 0.0 | 4.058 |
2 | 0 | 5 | 12 | 21.933 | 70.5 | 4.049 |
3 | 0 | 2 | 12 | 22.631 | 52.5 | 3.926 |
0 | 0 | 7 | 2 | 23.150 | 2.0 | 3.839 |
2 | 1 | 4 | 24 | 23.229 | 16.7 | 3.826 |
1 | 1 | 6 | 12 | 23.456 | 45.1 | 3.790 |
3 | 0 | 3 | 12 | 23.824 | 12.0 | 3.732 |
1 | 0 | 7 | 12 | 24.265 | 5.8 | 3.665 |
2 | 0 | 6 | 12 | 24.558 | 1.9 | 3.622 |
2 | 2 | 0 | 6 | 25.028 | 15.4 | 3.555 |
2 | 2 | 1 | 12 | 25.250 | 7.2 | 3.524 |
2 | 1 | 5 | 24 | 25.292 | 2.0 | 3.519 |
3 | 0 | 4 | 12 | 25.407 | 0.2 | 3.503 |
2 | 2 | 2 | 12 | 25.904 | 0.0 | 3.437 |
3 | 1 | 0 | 12 | 26.068 | 41.6 | 3.416 |
3 | 1 | 1 | 24 | 26.281 | 0.0 | 3.388 |
1 | 1 | 7 | 12 | 26.362 | 1.9 | 3.378 |
0 | 0 | 8 | 2 | 26.513 | 100.0 | 3.359 |
3 | 1 | 2 | 24 | 26.912 | 3.1 | 3.310 |
2 | 2 | 3 | 12 | 26.961 | 5.1 | 3.304 |
3 | 0 | 5 | 12 | 27.315 | 11.2 | 3.262 |
2 | 0 | 7 | 12 | 27.354 | 0.0 | 3.258 |
1 | 0 | 8 | 12 | 27.500 | 1.4 | 3.241 |
2 | 1 | 6 | 24 | 27.617 | 8.2 | 3.227 |
3 | 1 | 3 | 24 | 27.934 | 2.9 | 3.191 |
2 | 2 | 4 | 12 | 28.381 | 6.0 | 3.142 |
4 | 0 | 0 | 6 | 28.978 | 2.3 | 3.079 |
4 | 0 | 1 | 12 | 29.172 | 3.5 | 3.059 |
3 | 1 | 4 | 24 | 29.310 | 5.6 | 3.045 |
1 | 1 | 8 | 12 | 29.383 | 16.5 | 3.037 |
3 | 0 | 6 | 12 | 29.492 | 0.1 | 3.026 |
4 | 0 | 2 | 12 | 29.746 | 2.2 | 3.001 |
0 | 0 | 9 | 2 | 29.900 | 0.0 | 2.986 |
2 | 2 | 5 | 12 | 30.115 | 0.6 | 2.965 |
2 | 1 | 7 | 24 | 30.151 | 1.4 | 2.962 |
2 | 0 | 8 | 12 | 30.284 | 9.8 | 2.949 |
4 | 0 | 3 | 12 | 30.682 | 0.2 | 2.912 |
1 | 0 | 9 | 12 | 30.787 | 2.1 | 2.902 |
3 | 1 | 5 | 24 | 30.997 | 0.2 | 2.883 |
3 | 2 | 0 | 12 | 31.644 | 4.3 | 2.825 |
3 | 2 | 1 | 24 | 31.823 | 0.7 | 2.810 |
3 | 0 | 7 | 12 | 31.891 | 0.5 | 2.804 |
4 | 0 | 4 | 12 | 31.950 | 0.2 | 2.799 |
2 | 2 | 6 | 12 | 32.119 | 0.1 | 2.785 |
3 | 2 | 2 | 24 | 32.354 | 0.7 | 2.765 |
1 | 1 | 9 | 12 | 32.497 | 15.4 | 2.753 |
2 | 1 | 8 | 24 | 32.854 | 5.5 | 2.724 |
3 | 1 | 6 | 24 | 32.953 | 1.3 | 2.716 |
3 | 2 | 3 | 24 | 33.224 | 0.0 | 2.694 |
0 | 0 | 10 | 2 | 33.314 | 0.0 | 2.687 |
4 | 1 | 0 | 12 | 33.314 | 0.0 | 2.687 |
2 | 0 | 9 | 12 | 33.322 | 1.8 | 2.687 |
4 | 1 | 1 | 24 | 33.485 | 0.0 | 2.674 |
4 | 0 | 5 | 12 | 33.517 | 19.2 | 2.672 |
4 | 1 | 2 | 24 | 33.993 | 3.1 | 2.635 |
1 | 0 | 10 | 12 | 34.121 | 0.6 | 2.626 |
2 | 2 | 7 | 12 | 34.352 | 0.9 | 2.608 |
3 | 2 | 4 | 24 | 34.408 | 0.0 | 2.604 |
3 | 0 | 8 | 12 | 34.471 | 0.0 | 2.600 |
4 | 1 | 3 | 24 | 34.826 | 1.1 | 2.574 |
3 | 1 | 7 | 24 | 35.139 | 6.9 | 2.552 |
4 | 0 | 6 | 12 | 35.349 | 0.6 | 2.537 |
1 | 1 | 10 | 12 | 35.688 | 0.2 | 2.514 |
2 | 1 | 9 | 24 | 35.696 | 4.1 | 2.513 |
3 | 2 | 5 | 24 | 35.880 | 0.1 | 2.501 |
4 | 1 | 4 | 24 | 35.964 | 0.0 | 2.495 |
2 | 0 | 10 | 12 | 36.450 | 0.2 | 2.463 |
5 | 0 | 0 | 6 | 36.450 | 9.4 | 2.463 |
5 | 0 | 1 | 12 | 36.608 | 0.2 | 2.453 |
0 | 0 | 11 | 2 | 36.758 | 0.3 | 2.443 |
2 | 2 | 8 | 12 | 36.780 | 0.0 | 2.442 |
No data available
No 3D representation available
No data available
No data available