Synthesis
Mixture | Hydrated Prefer was dehydrated at 150°C |
SDA | 4-Amino-2,2,6,6-tetramethylpiperidine |
Temperature | 150.00 °C |
Duration | 6 h |
Conditions | n/a |
Reference |
Schreyeck, Caullet, Mougenel, Guth & Marler (1996): Microporous Materials, Volume 6, Issue 5-6, Pages 259-271. |
Crystal Structure
Structurally nearly identical materials | None |
Crystal chemically related materials | None |
Chemical composition per unit cell | (C9H22N2)4 [Si36O76] |
Lattice parameters of the 2D cell of the layer |
|
Lattice parameters related to the stacking direction |
|
Space group | Pnn2 |
XRD reflections representing the 2D cell of the layer |
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XRD reflections representing the layer-layer distance |
|
Reference |
Marler & Müller (2019): Microporous and Mesoporous Materials, Volume 288, Issue 1 November 2019, Pages 109597. |
Properties
Density (calculated) | 1.735 g/cm3 |
Condensation product | Silica-Ferrierite (zeolite framework type: FER) |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
0 | 2 | 0 | 2 | 6.720 | 100.0 | 13.143 |
1 | 1 | 0 | 4 | 7.138 | 3.1 | 12.374 |
1 | 2 | 0 | 4 | 9.214 | 0.2 | 9.590 |
1 | 3 | 0 | 4 | 11.900 | 0.3 | 7.431 |
0 | 1 | 1 | 4 | 12.377 | 9.8 | 7.146 |
2 | 0 | 0 | 2 | 12.613 | 1.9 | 7.013 |
2 | 1 | 0 | 4 | 13.056 | 0.4 | 6.776 |
0 | 4 | 0 | 2 | 13.464 | 5.1 | 6.571 |
1 | 0 | 1 | 4 | 13.482 | 4.7 | 6.562 |
1 | 1 | 1 | 8 | 13.898 | 0.2 | 6.367 |
2 | 2 | 0 | 4 | 14.304 | 2.5 | 6.187 |
1 | 4 | 0 | 4 | 14.876 | 0.1 | 5.951 |
1 | 2 | 1 | 8 | 15.078 | 3.9 | 5.871 |
0 | 3 | 1 | 4 | 15.631 | 6.4 | 5.665 |
2 | 3 | 0 | 4 | 16.176 | 0.1 | 5.475 |
. | . | . | . | . | . | |
1 | 3 | 1 | 8 | 16.866 | 0.0 | 5.252 |
2 | 1 | 1 | 8 | 17.706 | 3.1 | 5.005 |
1 | 5 | 0 | 4 | 18.006 | 5.0 | 4.923 |
2 | 4 | 0 | 4 | 18.489 | 13.3 | 4.795 |
2 | 2 | 1 | 8 | 18.653 | 0.0 | 4.753 |
1 | 4 | 1 | 8 | 19.098 | 5.1 | 4.643 |
3 | 1 | 0 | 4 | 19.268 | 0.2 | 4.603 |
2 | 3 | 1 | 8 | 20.135 | 2.4 | 4.407 |
3 | 2 | 0 | 4 | 20.144 | 0.0 | 4.405 |
0 | 6 | 0 | 2 | 20.254 | 1.8 | 4.381 |
0 | 5 | 1 | 4 | 20.685 | 1.1 | 4.291 |
2 | 5 | 0 | 4 | 21.104 | 1.3 | 4.206 |
1 | 6 | 0 | 4 | 21.230 | 0.5 | 4.182 |
3 | 3 | 0 | 4 | 21.527 | 2.2 | 4.125 |
1 | 5 | 1 | 8 | 21.643 | 0.1 | 4.103 |
2 | 4 | 1 | 8 | 22.049 | 0.3 | 4.028 |
3 | 0 | 1 | 4 | 22.455 | 4.9 | 3.956 |
3 | 1 | 1 | 8 | 22.711 | 0.5 | 3.912 |
3 | 4 | 0 | 4 | 23.333 | 1.0 | 3.809 |
3 | 2 | 1 | 8 | 23.464 | 0.3 | 3.788 |
2 | 6 | 0 | 4 | 23.931 | 3.2 | 3.715 |
0 | 0 | 2 | 2 | 23.949 | 1.0 | 3.713 |
2 | 5 | 1 | 8 | 24.300 | 11.8 | 3.660 |
1 | 6 | 1 | 8 | 24.410 | 3.8 | 3.644 |
1 | 7 | 0 | 4 | 24.522 | 2.1 | 3.627 |
3 | 3 | 1 | 8 | 24.671 | 0.1 | 3.606 |
0 | 2 | 2 | 4 | 24.901 | 13.5 | 3.573 |
1 | 1 | 2 | 8 | 25.021 | 4.6 | 3.556 |
4 | 0 | 0 | 2 | 25.382 | 8.0 | 3.506 |
3 | 5 | 0 | 4 | 25.476 | 7.2 | 3.493 |
4 | 1 | 0 | 4 | 25.610 | 2.9 | 3.476 |
1 | 2 | 2 | 8 | 25.710 | 0.0 | 3.462 |
3 | 4 | 1 | 8 | 26.273 | 0.3 | 3.389 |
4 | 2 | 0 | 4 | 26.285 | 5.4 | 3.388 |
0 | 7 | 1 | 4 | 26.580 | 1.4 | 3.351 |
2 | 6 | 1 | 8 | 26.810 | 0.2 | 3.323 |
1 | 3 | 2 | 8 | 26.822 | 7.6 | 3.321 |
2 | 7 | 0 | 4 | 26.912 | 0.2 | 3.310 |
0 | 8 | 0 | 2 | 27.118 | 0.5 | 3.286 |
2 | 0 | 2 | 4 | 27.155 | 0.1 | 3.281 |
1 | 7 | 1 | 8 | 27.342 | 0.1 | 3.259 |
2 | 1 | 2 | 8 | 27.370 | 0.0 | 3.256 |
4 | 3 | 0 | 4 | 27.375 | 0.2 | 3.255 |
0 | 4 | 2 | 4 | 27.573 | 7.7 | 3.232 |
1 | 8 | 0 | 4 | 27.867 | 0.1 | 3.199 |
3 | 6 | 0 | 4 | 27.887 | 0.6 | 3.197 |
2 | 2 | 2 | 8 | 28.005 | 1.2 | 3.183 |
3 | 5 | 1 | 8 | 28.208 | 0.1 | 3.161 |
1 | 4 | 2 | 8 | 28.310 | 0.0 | 3.150 |
4 | 1 | 1 | 8 | 28.330 | 0.3 | 3.148 |
4 | 4 | 0 | 4 | 28.838 | 0.6 | 3.093 |
4 | 2 | 1 | 8 | 28.946 | 0.1 | 3.082 |
2 | 3 | 2 | 8 | 29.036 | 0.0 | 3.073 |
2 | 7 | 1 | 8 | 29.520 | 1.0 | 3.023 |
4 | 3 | 1 | 8 | 29.947 | 0.2 | 2.981 |
2 | 8 | 0 | 4 | 30.010 | 0.3 | 2.975 |
1 | 5 | 2 | 8 | 30.125 | 2.3 | 2.964 |
1 | 8 | 1 | 8 | 30.400 | 0.4 | 2.938 |
3 | 6 | 1 | 8 | 30.419 | 0.4 | 2.936 |
2 | 4 | 2 | 8 | 30.425 | 0.1 | 2.936 |
3 | 7 | 0 | 4 | 30.510 | 0.4 | 2.928 |
4 | 5 | 0 | 4 | 30.624 | 0.1 | 2.917 |
3 | 1 | 2 | 8 | 30.919 | 1.4 | 2.890 |
1 | 9 | 0 | 4 | 31.258 | 0.4 | 2.859 |
4 | 4 | 1 | 8 | 31.299 | 0.0 | 2.856 |
3 | 2 | 2 | 8 | 31.489 | 0.1 | 2.839 |
0 | 6 | 2 | 4 | 31.562 | 0.2 | 2.832 |
5 | 1 | 0 | 4 | 32.064 | 0.0 | 2.789 |
2 | 5 | 2 | 8 | 32.131 | 0.1 | 2.784 |
1 | 6 | 2 | 8 | 32.217 | 0.1 | 2.776 |
2 | 8 | 1 | 8 | 32.391 | 0.1 | 2.762 |
3 | 3 | 2 | 8 | 32.419 | 0.9 | 2.759 |
5 | 2 | 0 | 4 | 32.616 | 0.0 | 2.743 |
4 | 6 | 0 | 4 | 32.687 | 0.3 | 2.737 |
3 | 7 | 1 | 8 | 32.858 | 0.1 | 2.724 |
0 | 9 | 1 | 4 | 32.929 | 0.0 | 2.718 |
4 | 5 | 1 | 8 | 32.964 | 0.1 | 2.715 |
2 | 9 | 0 | 4 | 33.203 | 0.0 | 2.696 |
3 | 8 | 0 | 4 | 33.303 | 0.0 | 2.688 |
5 | 3 | 0 | 4 | 33.517 | 0.1 | 2.671 |
1 | 9 | 1 | 8 | 33.559 | 0.0 | 2.668 |
3 | 4 | 2 | 8 | 33.682 | 0.0 | 2.659 |
0 | 10 | 0 | 2 | 34.082 | 0.0 | 2.629 |
2 | 6 | 2 | 8 | 34.112 | 1.4 | 2.626 |
5 | 0 | 1 | 4 | 34.142 | 1.1 | 2.624 |
5 | 1 | 1 | 8 | 34.317 | 0.5 | 2.611 |
1 | 7 | 2 | 8 | 34.542 | 0.5 | 2.595 |
1 | 10 | 0 | 4 | 34.694 | 0.0 | 2.584 |
5 | 4 | 0 | 4 | 34.745 | 0.2 | 2.580 |
5 | 2 | 1 | 8 | 34.837 | 0.0 | 2.573 |
4 | 6 | 1 | 8 | 34.904 | 0.0 | 2.568 |
4 | 7 | 0 | 4 | 34.984 | 0.0 | 2.563 |
4 | 0 | 2 | 4 | 35.177 | 0.2 | 2.549 |
3 | 5 | 2 | 8 | 35.247 | 0.0 | 2.544 |
4 | 1 | 2 | 8 | 35.347 | 0.1 | 2.537 |
2 | 9 | 1 | 8 | 35.391 | 0.0 | 2.534 |
3 | 8 | 1 | 8 | 35.487 | 0.2 | 2.528 |
5 | 3 | 1 | 8 | 35.689 | 0.1 | 2.514 |
4 | 2 | 2 | 8 | 35.854 | 0.7 | 2.503 |
3 | 9 | 0 | 4 | 36.237 | 0.1 | 2.477 |
5 | 5 | 0 | 4 | 36.270 | 0.6 | 2.475 |
2 | 7 | 2 | 8 | 36.331 | 0.1 | 2.471 |
0 | 1 | 3 | 4 | 36.431 | 0.3 | 2.464 |
2 | 10 | 0 | 4 | 36.476 | 0.0 | 2.461 |
0 | 8 | 2 | 4 | 36.488 | 0.5 | 2.460 |
Atom | x | y | z | Biso | Occ. | |
---|---|---|---|---|---|---|
Si1 | 0.2238 | 0.3022 | 0.2410 | 1.30 | 1.000 | |
Si7 | 0.2841 | 0.7932 | 0.3220 | 1.30 | 1.000 | |
Si2 | 0.8091 | 0.3046 | 0.8220 | 1.30 | 1.000 | |
Si8 | 0.6900 | 0.8137 | 0.7450 | 1.30 | 1.000 | |
Si3 | 0.0126 | 0.2674 | 0.3240 | 1.30 | 1.000 | |
Si9 | 0.4885 | 0.7640 | 0.2480 | 1.30 | 1.000 | |
Si4 | 0.8097 | 0.1328 | 0.0330 | 1.30 | 1.000 | |
Si5 | 0.2154 | 0.1215 | 0.0350 | 1.30 | 1.000 | |
Si6 | -0.0179 | 0.8183 | 0.0300 | 1.30 | 1.000 | |
O1 | 0.5110 | 0.2489 | 0.0360 | 1.30 | 1.000 | |
O2 | 0.8000 | 0.0738 | 0.0480 | 1.30 | 1.000 | |
O3 | 0.2180 | 0.0632 | 0.0550 | 1.30 | 1.000 | |
O4 | 0.9198 | 0.1490 | 0.0240 | 1.30 | 1.000 | |
O5 | 0.1100 | 0.1444 | 0.0330 | 1.30 | 1.000 | |
O6 | 0.2810 | 0.2523 | 0.2850 | 1.30 | 1.000 | |
O14 | 0.2400 | 0.7384 | 0.2970 | 1.30 | 1.000 | |
O7 | 0.5430 | 0.2859 | 0.3470 | 1.30 | 1.000 | |
O15 | 0.0020 | 0.7822 | 0.2060 | 1.30 | 1.000 | |
O8 | 0.2050 | 0.6749 | 0.0300 | 1.30 | 1.000 | |
O9 | 0.7590 | 0.6837 | 0.0260 | 1.30 | 1.000 | |
O10 | 0.2570 | 0.3524 | 0.3420 | 1.30 | 1.000 | |
O16 | 0.2250 | 0.8301 | 0.1930 | 1.30 | 1.000 | |
O11 | 0.7730 | 0.3478 | 0.6880 | 1.30 | 1.000 | |
O17 | 0.7180 | 0.8629 | 0.8630 | 1.30 | 1.000 | |
O12 | 0.1130 | 0.2950 | 0.2870 | 1.30 | 1.000 | |
O18 | 0.3970 | 0.8009 | 0.2790 | 1.30 | 1.000 | |
O13 | 0.9220 | 0.3000 | 0.7850 | 1.30 | 1.000 | |
O19 | 0.5790 | 0.8057 | 0.7940 | 1.30 | 1.000 | |
C11 | -0.0730 | -0.0918 | 0.5520 | 32.80 | 0.750 | |
C21 | -0.0062 | -0.0476 | 0.5990 | 32.80 | 0.500 | |
C31 | 0.0910 | -0.0573 | 0.5090 | 32.80 | 0.750 | |
C41 | 0.0070 | -0.0452 | 0.8040 | 32.80 | 0.667 | |
C51 | 0.0790 | -0.0032 | 0.8490 | 32.80 | 0.583 | |
N21 | 0.0960 | -0.0020 | 1.0420 | 32.80 | 0.714 | |
N11 | -0.0450 | 0.0003 | 0.5330 | 32.80 | 0.643 | |
C81 | 0.0100 | 0.0450 | 0.5810 | 32.80 | 0.500 | |
C91 | 0.0340 | 0.0462 | 0.7810 | 32.80 | 0.667 | |
C61 | 0.0990 | 0.0494 | 0.4660 | 32.80 | 0.750 | |
C71 | -0.0450 | 0.0934 | 0.5300 | 32.80 | 0.750 | |
C12 | 0.1660 | 0.5065 | 0.3900 | 32.80 | 0.750 | |
C22 | 0.0920 | 0.4961 | 0.5450 | 32.80 | 0.500 | |
C32 | -0.0230 | 0.5439 | 0.4630 | 32.80 | 0.750 | |
C42 | 0.0360 | 0.5450 | 0.5740 | 32.80 | 0.667 | |
C52 | -0.0110 | 0.5448 | 0.7620 | 32.80 | 0.583 | |
N22 | -0.0660 | 0.5910 | 0.7890 | 32.80 | 0.714 | |
N12 | 0.1400 | 0.4777 | 0.7000 | 32.80 | 0.643 | |
C82 | 0.1129 | 0.4896 | 0.8810 | 32.80 | 0.500 | |
C92 | 0.0760 | 0.5451 | 0.8950 | 32.80 | 0.667 | |
C62 | 0.0290 | 0.4558 | 0.9450 | 32.80 | 0.750 | |
C72 | 0.1940 | 0.4840 | 1.0180 | 32.80 | 0.750 |
User Cell Range (natural numbers 1-5):
No data available