Synthesis
Mixture | 1 SiO2 : 2.8 SDA : 55 H2O |
SDA | Tetramethylammonium hydroxide |
Temperature | 160.00 °C |
Duration | 18 d |
Conditions | static |
Reference |
Marler, Wang, Song & Gies (2014): Dalton Transactions, Volume 43, Issue 27, Pages 10396-10416. |
Crystal Structure
Properties
Density (calculated) | 1.975 g/cm3 |
Condensation product | highly disordered |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
1 | 0 | 0 | 2 | 8.499 | 100.0 | 10.396 |
1 | 1 | 0 | 4 | 10.594 | 0.1 | 8.344 |
0 | 0 | 1 | 2 | 12.043 | 1.3 | 7.343 |
0 | 2 | 0 | 2 | 12.647 | 5.6 | 6.994 |
0 | 1 | 1 | 4 | 13.609 | 6.1 | 6.501 |
-1 | 0 | 1 | 2 | 13.777 | 14.3 | 6.422 |
-1 | 1 | 1 | 4 | 15.168 | 2.9 | 5.837 |
1 | 2 | 0 | 4 | 15.256 | 2.5 | 5.803 |
1 | 0 | 1 | 2 | 15.679 | 3.1 | 5.647 |
1 | 1 | 1 | 4 | 16.918 | 0.1 | 5.237 |
2 | 0 | 0 | 2 | 17.045 | 1.0 | 5.198 |
0 | 2 | 1 | 4 | 17.498 | 0.9 | 5.064 |
2 | 1 | 0 | 4 | 18.193 | 11.6 | 4.872 |
-1 | 2 | 1 | 4 | 18.743 | 5.1 | 4.730 |
-2 | 0 | 1 | 2 | 19.523 | 0.2 | 4.543 |
. | . | . | . | . | . | |
1 | 2 | 1 | 4 | 20.194 | 8.1 | 4.394 |
-2 | 1 | 1 | 4 | 20.538 | 9.2 | 4.321 |
1 | 3 | 0 | 4 | 20.864 | 10.8 | 4.254 |
2 | 2 | 0 | 4 | 21.280 | 33.9 | 4.172 |
2 | 0 | 1 | 2 | 22.237 | 3.2 | 3.995 |
0 | 3 | 1 | 4 | 22.571 | 18.2 | 3.936 |
2 | 1 | 1 | 4 | 23.138 | 14.9 | 3.841 |
-2 | 2 | 1 | 4 | 23.329 | 15.6 | 3.810 |
-1 | 3 | 1 | 4 | 23.560 | 0.6 | 3.773 |
0 | 0 | 2 | 2 | 24.223 | 4.3 | 3.671 |
-1 | 0 | 2 | 2 | 24.575 | 11.7 | 3.620 |
1 | 3 | 1 | 4 | 24.742 | 0.4 | 3.595 |
0 | 1 | 2 | 4 | 25.056 | 7.0 | 3.551 |
-1 | 1 | 2 | 4 | 25.398 | 12.6 | 3.504 |
0 | 4 | 0 | 2 | 25.451 | 23.2 | 3.497 |
2 | 3 | 0 | 4 | 25.646 | 19.6 | 3.471 |
2 | 2 | 1 | 4 | 25.662 | 9.0 | 3.469 |
3 | 0 | 0 | 2 | 25.687 | 2.4 | 3.465 |
3 | 1 | 0 | 4 | 26.478 | 4.2 | 3.364 |
1 | 0 | 2 | 2 | 26.806 | 14.0 | 3.323 |
1 | 4 | 0 | 4 | 26.878 | 5.4 | 3.314 |
-3 | 0 | 1 | 2 | 26.897 | 2.4 | 3.312 |
-2 | 3 | 1 | 4 | 27.387 | 0.0 | 3.254 |
0 | 2 | 2 | 4 | 27.415 | 0.3 | 3.251 |
1 | 1 | 2 | 4 | 27.567 | 6.4 | 3.233 |
-3 | 1 | 1 | 4 | 27.655 | 1.3 | 3.223 |
-1 | 2 | 2 | 4 | 27.729 | 0.4 | 3.215 |
-2 | 0 | 2 | 2 | 27.759 | 8.3 | 3.211 |
0 | 4 | 1 | 4 | 28.244 | 0.3 | 3.157 |
-2 | 1 | 2 | 4 | 28.496 | 6.0 | 3.130 |
3 | 2 | 0 | 4 | 28.728 | 2.5 | 3.105 |
-1 | 4 | 1 | 4 | 29.052 | 3.7 | 3.071 |
2 | 3 | 1 | 4 | 29.421 | 0.0 | 3.033 |
1 | 2 | 2 | 4 | 29.741 | 0.0 | 3.002 |
-3 | 2 | 1 | 4 | 29.824 | 0.4 | 2.993 |
3 | 0 | 1 | 2 | 29.945 | 0.4 | 2.982 |
1 | 4 | 1 | 4 | 30.032 | 0.9 | 2.973 |
-2 | 2 | 2 | 4 | 30.610 | 0.5 | 2.918 |
3 | 1 | 1 | 4 | 30.634 | 0.5 | 2.916 |
2 | 4 | 0 | 4 | 30.792 | 2.0 | 2.901 |
0 | 3 | 2 | 4 | 30.977 | 2.3 | 2.884 |
-1 | 3 | 2 | 4 | 31.259 | 1.9 | 2.859 |
2 | 0 | 2 | 2 | 31.662 | 0.1 | 2.824 |
3 | 3 | 0 | 4 | 32.158 | 0.3 | 2.781 |
-2 | 4 | 1 | 4 | 32.279 | 0.0 | 2.771 |
2 | 1 | 2 | 4 | 32.318 | 0.5 | 2.768 |
3 | 2 | 1 | 4 | 32.623 | 0.4 | 2.743 |
-3 | 0 | 2 | 2 | 33.023 | 1.0 | 2.710 |
1 | 3 | 2 | 4 | 33.076 | 0.3 | 2.706 |
1 | 5 | 0 | 4 | 33.135 | 0.0 | 2.701 |
-3 | 3 | 1 | 4 | 33.151 | 1.0 | 2.700 |
-3 | 1 | 2 | 4 | 33.655 | 0.7 | 2.661 |
-2 | 3 | 2 | 4 | 33.868 | 0.4 | 2.645 |
2 | 4 | 1 | 4 | 34.047 | 0.1 | 2.631 |
2 | 2 | 2 | 4 | 34.219 | 0.8 | 2.618 |
0 | 5 | 1 | 4 | 34.274 | 2.7 | 2.614 |
4 | 0 | 0 | 2 | 34.482 | 0.0 | 2.599 |
-1 | 5 | 1 | 4 | 34.956 | 0.6 | 2.565 |
-4 | 0 | 1 | 2 | 34.998 | 0.0 | 2.562 |
4 | 1 | 0 | 4 | 35.091 | 0.0 | 2.555 |
0 | 4 | 2 | 4 | 35.421 | 0.4 | 2.532 |
-3 | 2 | 2 | 4 | 35.493 | 2.1 | 2.527 |
-4 | 1 | 1 | 4 | 35.599 | 0.2 | 2.520 |
-1 | 4 | 2 | 4 | 35.672 | 0.0 | 2.515 |
3 | 3 | 1 | 4 | 35.717 | 0.2 | 2.512 |
1 | 5 | 1 | 4 | 35.791 | 0.5 | 2.507 |
2 | 5 | 0 | 4 | 36.444 | 0.8 | 2.463 |
3 | 4 | 0 | 4 | 36.474 | 0.1 | 2.461 |
-1 | 0 | 3 | 2 | 36.526 | 0.4 | 2.458 |
0 | 0 | 3 | 2 | 36.687 | 1.4 | 2.448 |
4 | 2 | 0 | 4 | 36.866 | 0.1 | 2.436 |
Atom | x | y | z | Biso | Occ. | |
---|---|---|---|---|---|---|
Si1 | 0.8044 | 0.9521 | 0.3053 | 1.54 | 1.000 | |
Si2 | 0.4682 | 0.7500 | 0.5408 | 1.54 | 0.500 | |
Si3 | 0.6359 | 0.0472 | 0.9823 | 1.54 | 1.000 | |
Si4 | 0.4582 | 0.7500 | 0.9517 | 1.54 | 0.500 | |
Si5 | 0.6285 | 0.0543 | 0.5678 | 1.54 | 0.522 | |
Si52 | 0.7142 | 0.0782 | 0.6028 | 1.54 | 0.478 | |
Si6 | 0.3241 | 0.2500 | 0.7150 | 1.54 | 0.500 | |
O1 | 0.6121 | 0.1567 | 0.5197 | 2.58 | 1.000 | |
O2 | 0.5000 | 0.5000 | 0.0000 | 2.58 | 0.500 | |
O3 | 0.7700 | 0.8374 | 0.2960 | 2.58 | 1.000 | |
O4 | 0.6309 | 0.1595 | 0.0212 | 2.58 | 1.000 | |
O5 | 0.6702 | 0.0328 | 0.7807 | 2.58 | 1.000 | |
O6 | 0.9609 | 0.9705 | 0.3483 | 2.58 | 1.000 | |
O7 | 0.5982 | 0.7500 | 0.4555 | 2.58 | 0.500 | |
O8 | 0.5814 | 0.7500 | 0.0952 | 2.58 | 0.500 | |
O9 | 0.5158 | 0.7500 | 0.7583 | 2.58 | 0.500 | |
O10 | 0.7264 | -0.0008 | 0.4571 | 2.58 | 1.000 | |
O11 | 0.7457 | -0.0005 | 0.1121 | 2.58 | 1.000 | |
O12 | 0.5000 | 0.5000 | 0.5000 | 2.58 | 0.266 | |
N1 | -0.0275 | 0.7500 | 0.8347 | 1.71 | 0.422 | |
C1 | -0.1169 | 0.6744 | 0.8240 | 13.36 | 1.266 | |
C2 | 0.0457 | 0.7500 | 1.0157 | 13.36 | 0.633 | |
C3 | 0.0628 | 0.7500 | 0.7013 | 13.36 | 0.633 | |
F1 | -0.1462 | 0.1190 | 0.6483 | 5.46 | 0.540 |
User Cell Range (natural numbers 1-5):