Synthesis
Mixture | 0.5 SDA : 1 SiO2 : 10 H2O |
SDA | Diethyldimethylammonium hydroxide |
Temperature | 150.00 °C |
Duration | 15 d |
Conditions | static |
Reference |
Marler, Wang, Song & Gies (2014): Dalton Transactions, Volume 43, Issue 27, Pages 10396-10416. |
Crystal Structure
Structurally nearly identical materials | |
Crystal chemically related materials | None |
Chemical composition per unit cell | [(CH3)2(C2H5)2N]4 [Si36O72(OH)4] |
Lattice parameters of the 2D cell of the layer |
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Lattice parameters related to the stacking direction |
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Space group | Pna2(1) |
XRD reflections representing the 2D cell of the layer |
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XRD reflections representing the layer-layer distance |
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Reference |
Marler, Wang, Song & Gies (2014): Dalton Transactions, Volume 43, Issue 27, Pages 10396-10416. |
Properties
Density (calculated) | 1.899 g/cm3 |
Condensation product | RUB-37, UZM-25 [38] (zeolite framework type: CDO) |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
2 | 0 | 0 | 2 | 7.961 | 100.0 | 11.097 |
2 | 1 | 0 | 4 | 10.165 | 0.5 | 8.695 |
1 | 0 | 1 | 4 | 12.636 | 6.2 | 7.000 |
0 | 2 | 0 | 2 | 12.639 | 2.4 | 6.998 |
0 | 1 | 1 | 4 | 13.559 | 0.5 | 6.525 |
1 | 1 | 1 | 8 | 14.136 | 8.0 | 6.260 |
2 | 0 | 1 | 4 | 14.408 | 1.4 | 6.143 |
2 | 2 | 0 | 4 | 14.954 | 0.2 | 5.919 |
2 | 1 | 1 | 8 | 15.742 | 0.4 | 5.625 |
4 | 0 | 0 | 2 | 15.961 | 0.5 | 5.548 |
3 | 0 | 1 | 4 | 16.961 | 6.3 | 5.223 |
4 | 1 | 0 | 4 | 17.178 | 6.4 | 5.158 |
1 | 2 | 1 | 8 | 17.909 | 6.2 | 4.949 |
3 | 1 | 1 | 8 | 18.113 | 2.6 | 4.894 |
2 | 2 | 1 | 8 | 19.210 | 0.1 | 4.617 |
. | . | . | . | . | . | |
4 | 0 | 1 | 4 | 20.009 | 0.3 | 4.434 |
4 | 2 | 0 | 4 | 20.410 | 18.7 | 4.348 |
2 | 3 | 0 | 4 | 20.635 | 2.1 | 4.301 |
4 | 1 | 1 | 8 | 21.000 | 1.5 | 4.227 |
3 | 2 | 1 | 8 | 21.208 | 12.4 | 4.186 |
0 | 3 | 1 | 4 | 22.532 | 1.4 | 3.943 |
1 | 3 | 1 | 8 | 22.889 | 5.1 | 3.882 |
5 | 0 | 1 | 4 | 23.371 | 4.4 | 3.803 |
4 | 2 | 1 | 8 | 23.736 | 1.2 | 3.745 |
2 | 3 | 1 | 8 | 23.932 | 0.2 | 3.715 |
6 | 0 | 0 | 2 | 24.039 | 3.2 | 3.699 |
0 | 0 | 2 | 2 | 24.112 | 1.5 | 3.688 |
5 | 1 | 1 | 8 | 24.231 | 4.9 | 3.670 |
1 | 0 | 2 | 4 | 24.447 | 3.4 | 3.638 |
6 | 1 | 0 | 4 | 24.878 | 6.3 | 3.576 |
4 | 3 | 0 | 4 | 24.915 | 16.8 | 3.571 |
1 | 1 | 2 | 8 | 25.273 | 2.9 | 3.521 |
2 | 0 | 2 | 4 | 25.430 | 12.3 | 3.500 |
0 | 4 | 0 | 2 | 25.435 | 21.5 | 3.499 |
3 | 3 | 1 | 8 | 25.580 | 1.0 | 3.480 |
2 | 1 | 2 | 8 | 26.226 | 8.5 | 3.395 |
5 | 2 | 1 | 8 | 26.655 | 10.1 | 3.342 |
2 | 4 | 0 | 4 | 26.692 | 5.5 | 3.337 |
6 | 0 | 1 | 4 | 26.944 | 0.0 | 3.306 |
3 | 0 | 2 | 4 | 26.992 | 9.5 | 3.301 |
6 | 2 | 0 | 4 | 27.248 | 2.4 | 3.270 |
0 | 2 | 2 | 4 | 27.312 | 0.2 | 3.263 |
1 | 2 | 2 | 8 | 27.611 | 0.5 | 3.228 |
6 | 1 | 1 | 8 | 27.700 | 0.5 | 3.218 |
4 | 3 | 1 | 8 | 27.734 | 0.1 | 3.214 |
3 | 1 | 2 | 8 | 27.747 | 5.1 | 3.213 |
2 | 2 | 2 | 8 | 28.492 | 0.9 | 3.130 |
1 | 4 | 1 | 8 | 28.496 | 0.3 | 3.130 |
4 | 0 | 2 | 4 | 29.049 | 2.0 | 3.071 |
2 | 4 | 1 | 8 | 29.352 | 0.0 | 3.040 |
4 | 1 | 2 | 8 | 29.756 | 1.6 | 3.000 |
6 | 2 | 1 | 8 | 29.863 | 0.1 | 2.990 |
3 | 2 | 2 | 8 | 29.907 | 0.2 | 2.985 |
4 | 4 | 0 | 4 | 30.171 | 0.7 | 2.960 |
5 | 3 | 1 | 8 | 30.296 | 0.6 | 2.948 |
7 | 0 | 1 | 4 | 30.669 | 0.1 | 2.913 |
3 | 4 | 1 | 8 | 30.731 | 0.3 | 2.907 |
6 | 3 | 0 | 4 | 30.824 | 0.8 | 2.898 |
1 | 3 | 2 | 8 | 31.149 | 1.5 | 2.869 |
7 | 1 | 1 | 8 | 31.342 | 0.6 | 2.852 |
5 | 0 | 2 | 4 | 31.513 | 0.0 | 2.837 |
4 | 2 | 2 | 8 | 31.791 | 0.5 | 2.812 |
2 | 3 | 2 | 8 | 31.941 | 1.0 | 2.800 |
5 | 1 | 2 | 8 | 32.171 | 0.9 | 2.780 |
8 | 0 | 0 | 2 | 32.242 | 0.1 | 2.774 |
4 | 4 | 1 | 8 | 32.572 | 0.0 | 2.747 |
8 | 1 | 0 | 4 | 32.887 | 0.1 | 2.721 |
2 | 5 | 0 | 4 | 32.974 | 0.0 | 2.714 |
6 | 3 | 1 | 8 | 33.182 | 0.1 | 2.698 |
3 | 3 | 2 | 8 | 33.223 | 0.0 | 2.695 |
7 | 2 | 1 | 8 | 33.290 | 0.3 | 2.689 |
5 | 2 | 2 | 8 | 34.077 | 0.4 | 2.629 |
0 | 5 | 1 | 4 | 34.235 | 0.3 | 2.617 |
6 | 0 | 2 | 4 | 34.308 | 0.2 | 2.612 |
1 | 5 | 1 | 8 | 34.479 | 2.0 | 2.599 |
8 | 0 | 1 | 4 | 34.514 | 0.0 | 2.597 |
8 | 2 | 0 | 4 | 34.757 | 0.0 | 2.579 |
5 | 4 | 1 | 8 | 34.812 | 0.0 | 2.575 |
6 | 1 | 2 | 8 | 34.919 | 0.5 | 2.567 |
4 | 3 | 2 | 8 | 34.947 | 0.0 | 2.565 |
8 | 1 | 1 | 8 | 35.121 | 0.1 | 2.553 |
2 | 5 | 1 | 8 | 35.204 | 0.0 | 2.547 |
6 | 4 | 0 | 4 | 35.280 | 0.1 | 2.542 |
0 | 4 | 2 | 4 | 35.331 | 0.5 | 2.538 |
1 | 4 | 2 | 8 | 35.569 | 0.4 | 2.522 |
4 | 5 | 0 | 4 | 35.904 | 1.4 | 2.499 |
2 | 4 | 2 | 8 | 36.275 | 0.7 | 2.474 |
7 | 3 | 1 | 8 | 36.331 | 0.6 | 2.471 |
3 | 5 | 1 | 8 | 36.384 | 0.6 | 2.467 |
6 | 2 | 2 | 8 | 36.699 | 1.3 | 2.447 |
1 | 0 | 3 | 4 | 36.747 | 0.0 | 2.444 |
8 | 2 | 1 | 8 | 36.893 | 0.1 | 2.434 |
Atom | x | y | z | Biso | Occ. | |
---|---|---|---|---|---|---|
Si11 | 0.1709 | 0.2638 | 0.0599 | 1.09 | 1.000 | |
Si21 | 0.1117 | 0.4689 | 0.0595 | 1.09 | 1.000 | |
Si22 | 0.3984 | 0.5656 | 0.5672 | 1.09 | 1.000 | |
Si31 | 0.2726 | 0.2719 | 0.3432 | 1.09 | 1.000 | |
Si34 | 0.2651 | 0.2670 | 0.7651 | 1.09 | 1.000 | |
Si41 | 0.3201 | 0.4737 | 0.2634 | 1.09 | 1.000 | |
Si42 | 0.1889 | 0.5668 | 0.7614 | 1.09 | 1.000 | |
Si44 | 0.3047 | 1.0647 | 0.8562 | 1.09 | 1.000 | |
Si45 | 0.1875 | 0.9745 | 0.3468 | 1.09 | 1.000 | |
O11 | 0.0305 | 1.0551 | 0.0726 | 1.98 | 1.000 | |
O12 | 0.4597 | 0.9593 | 0.5696 | 1.98 | 1.000 | |
O21 | 0.2528 | 0.2687 | 0.5512 | 1.98 | 1.000 | |
O31 | 0.1275 | 0.3545 | 0.0413 | 1.98 | 1.000 | |
O32 | 0.3748 | 0.6754 | 0.5818 | 1.98 | 1.000 | |
O41 | 0.2144 | 0.2732 | 0.2225 | 1.98 | 1.000 | |
O44 | 0.2051 | 0.2646 | 0.8754 | 1.98 | 1.000 | |
O51 | 0.2591 | 0.5258 | 0.3174 | 1.98 | 1.000 | |
O52 | 0.2531 | 0.5267 | 0.8000 | 1.98 | 1.000 | |
O61 | 0.1694 | 0.5527 | 0.5545 | 1.98 | 1.000 | |
O62 | 0.3322 | 0.4836 | 0.0526 | 1.98 | 1.000 | |
O71 | 0.1476 | 0.5136 | 0.2265 | 1.98 | 1.000 | |
O72 | 0.3696 | 0.5076 | 0.7348 | 1.98 | 1.000 | |
O74 | 0.1269 | 1.0246 | 0.8773 | 1.98 | 1.000 | |
O75 | 0.3651 | 0.0224 | 0.3816 | 1.98 | 1.000 | |
O81 | 0.3165 | 0.3594 | 0.3150 | 1.98 | 1.000 | |
O82 | 0.1877 | 0.6806 | 0.8095 | 1.98 | 1.000 | |
O83 | 0.3078 | 1.1759 | 0.7995 | 1.98 | 1.000 | |
O84 | 0.1960 | 0.8597 | 0.3162 | 1.98 | 1.000 | |
N1 | 0.4856 | 0.7254 | 0.0699 | 28.25 | 1.000 | |
C1 | 0.4900 | 0.7945 | -0.0850 | 28.25 | 1.333 | |
C2 | 0.5399 | 0.7619 | 0.1659 | 28.25 | 1.333 | |
C3 | 0.5357 | 0.7820 | 0.3713 | 28.25 | 1.500 | |
C4 | 0.5494 | 0.7750 | -0.1820 | 28.25 | 1.500 | |
C5 | 0.4982 | 0.6212 | 0.0380 | 28.25 | 1.500 | |
C6 | 0.4215 | 0.7500 | 0.1060 | 28.25 | 1.500 |
User Cell Range (natural numbers 1-5):