Synthesis
Mixture | 0.55 SDA : 1 SiO2 : 8-12 H2O |
SDA | Dimethyldipropylammonium hydroxide |
Temperature | 150.00 °C |
Duration | 21 d |
Conditions | rotated |
Reference |
Grünewald-Lüke, Gies, Müller, Yilmaz, Imai, Tatsumi, Xie, Xiao, Bao, Zhang & De Vos (2012): Microporous and Mesoporous Materials, Volume 147, Issue 1, Pages 102-109. |
Crystal Structure
Structurally nearly identical materials | None |
Crystal chemically related materials | |
Chemical composition per unit cell | (C8H20N)2 [Si18O36(OH)2] ∙ x H2O |
Lattice parameters of the 2D cell of the layer |
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Lattice parameters related to the stacking direction |
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Space group | P2/c |
XRD reflections representing the 2D cell of the layer |
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XRD reflections representing the layer-layer distance |
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Reference |
Wang, Gies & Lin (2007): Chemistry of Materials, Volume 19, Issue 17, Pages 4181–4188. |
Properties
Density (calculated) | 1.839 g/cm3 |
Condensation product | RUB-41 (zeolite framework type RRO) |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
0 | 1 | 0 | 2 | 8.246 | 100.0 | 10.714 |
0 | 1 | 1 | 4 | 9.972 | 0.0 | 8.863 |
0 | 0 | 2 | 2 | 11.209 | 6.2 | 7.887 |
-1 | 0 | 2 | 2 | 13.221 | 0.7 | 6.691 |
1 | 0 | 0 | 2 | 13.390 | 9.0 | 6.607 |
0 | 1 | 2 | 4 | 13.931 | 1.0 | 6.352 |
-1 | 1 | 1 | 4 | 14.628 | 3.7 | 6.051 |
-1 | 1 | 2 | 4 | 15.602 | 1.0 | 5.675 |
1 | 1 | 0 | 4 | 15.745 | 2.4 | 5.624 |
0 | 2 | 0 | 2 | 16.535 | 2.3 | 5.357 |
0 | 2 | 1 | 4 | 17.470 | 0.3 | 5.072 |
-1 | 1 | 3 | 4 | 18.344 | 4.1 | 4.833 |
1 | 1 | 1 | 4 | 18.588 | 6.2 | 4.770 |
0 | 1 | 3 | 4 | 18.784 | 1.1 | 4.720 |
0 | 2 | 2 | 4 | 20.021 | 16.1 | 4.431 |
. | . | . | . | . | . | |
-1 | 2 | 1 | 4 | 20.517 | 4.1 | 4.325 |
-1 | 0 | 4 | 2 | 20.607 | 0.3 | 4.307 |
1 | 0 | 2 | 2 | 20.934 | 0.1 | 4.240 |
-1 | 2 | 2 | 4 | 21.229 | 2.8 | 4.182 |
1 | 2 | 0 | 4 | 21.336 | 0.8 | 4.161 |
-1 | 1 | 4 | 4 | 22.229 | 13.8 | 3.996 |
0 | 0 | 4 | 2 | 22.527 | 0.9 | 3.944 |
1 | 1 | 2 | 4 | 22.534 | 4.1 | 3.943 |
-1 | 2 | 3 | 4 | 23.340 | 0.9 | 3.808 |
1 | 2 | 1 | 4 | 23.535 | 19.0 | 3.777 |
0 | 2 | 3 | 4 | 23.691 | 16.8 | 3.753 |
0 | 1 | 4 | 4 | 24.026 | 0.4 | 3.701 |
-2 | 0 | 2 | 2 | 24.259 | 0.8 | 3.666 |
0 | 3 | 0 | 2 | 24.912 | 0.5 | 3.571 |
0 | 3 | 1 | 4 | 25.553 | 0.0 | 3.483 |
-2 | 1 | 2 | 4 | 25.662 | 8.1 | 3.469 |
-2 | 1 | 3 | 4 | 26.199 | 2.7 | 3.399 |
-2 | 1 | 1 | 4 | 26.374 | 0.8 | 3.377 |
-1 | 2 | 4 | 4 | 26.535 | 1.7 | 3.356 |
-2 | 0 | 4 | 2 | 26.623 | 3.9 | 3.346 |
1 | 2 | 2 | 4 | 26.794 | 0.7 | 3.325 |
-1 | 1 | 5 | 4 | 26.794 | 0.2 | 3.325 |
2 | 0 | 0 | 2 | 26.966 | 3.8 | 3.304 |
1 | 1 | 3 | 4 | 27.135 | 2.0 | 3.284 |
0 | 3 | 2 | 4 | 27.392 | 0.8 | 3.253 |
-1 | 3 | 1 | 4 | 27.764 | 0.0 | 3.211 |
-2 | 1 | 4 | 4 | 27.916 | 5.4 | 3.193 |
0 | 2 | 4 | 4 | 28.074 | 0.0 | 3.176 |
2 | 1 | 0 | 4 | 28.245 | 0.0 | 3.157 |
-1 | 3 | 2 | 4 | 28.304 | 1.0 | 3.151 |
1 | 3 | 0 | 4 | 28.385 | 0.6 | 3.142 |
0 | 1 | 5 | 4 | 29.491 | 0.9 | 3.026 |
-2 | 2 | 2 | 4 | 29.501 | 1.4 | 3.025 |
-1 | 3 | 3 | 4 | 29.948 | 1.0 | 2.981 |
-2 | 2 | 3 | 4 | 29.974 | 0.7 | 2.979 |
1 | 3 | 1 | 4 | 30.103 | 2.9 | 2.966 |
-2 | 2 | 1 | 4 | 30.129 | 1.4 | 2.964 |
0 | 3 | 3 | 4 | 30.228 | 2.3 | 2.954 |
-1 | 2 | 5 | 4 | 30.501 | 1.9 | 2.928 |
-2 | 1 | 5 | 4 | 30.631 | 2.0 | 2.916 |
-1 | 0 | 6 | 2 | 30.640 | 0.7 | 2.916 |
1 | 2 | 3 | 4 | 30.805 | 0.0 | 2.900 |
1 | 0 | 4 | 2 | 31.017 | 0.1 | 2.881 |
2 | 1 | 1 | 4 | 31.084 | 1.6 | 2.875 |
-2 | 2 | 4 | 4 | 31.502 | 0.1 | 2.838 |
-1 | 1 | 6 | 4 | 31.783 | 0.8 | 2.813 |
2 | 2 | 0 | 4 | 31.797 | 1.3 | 2.812 |
1 | 1 | 4 | 4 | 32.148 | 0.1 | 2.782 |
-1 | 3 | 4 | 4 | 32.545 | 0.3 | 2.749 |
1 | 3 | 2 | 4 | 32.760 | 0.0 | 2.731 |
0 | 2 | 5 | 4 | 32.921 | 3.5 | 2.718 |
-2 | 0 | 6 | 2 | 33.060 | 0.3 | 2.707 |
0 | 4 | 0 | 2 | 33.428 | 0.0 | 2.678 |
2 | 0 | 2 | 2 | 33.624 | 0.0 | 2.663 |
0 | 3 | 4 | 4 | 33.835 | 0.1 | 2.647 |
0 | 4 | 1 | 4 | 33.921 | 0.0 | 2.641 |
-2 | 2 | 5 | 4 | 33.958 | 0.0 | 2.638 |
0 | 0 | 6 | 2 | 34.074 | 0.0 | 2.629 |
-2 | 1 | 6 | 4 | 34.131 | 0.0 | 2.625 |
2 | 2 | 1 | 4 | 34.371 | 0.2 | 2.607 |
2 | 1 | 2 | 4 | 34.679 | 0.2 | 2.585 |
-1 | 2 | 6 | 4 | 35.012 | 0.0 | 2.561 |
-2 | 3 | 2 | 4 | 35.050 | 0.0 | 2.558 |
0 | 1 | 6 | 4 | 35.117 | 0.0 | 2.553 |
1 | 2 | 4 | 4 | 35.348 | 0.3 | 2.537 |
0 | 4 | 2 | 4 | 35.363 | 0.6 | 2.536 |
-2 | 3 | 3 | 4 | 35.456 | 0.3 | 2.530 |
-2 | 3 | 1 | 4 | 35.589 | 0.9 | 2.521 |
-1 | 4 | 1 | 4 | 35.658 | 0.0 | 2.516 |
-1 | 3 | 5 | 4 | 35.911 | 0.1 | 2.499 |
-1 | 4 | 2 | 4 | 36.092 | 1.3 | 2.487 |
1 | 4 | 0 | 4 | 36.157 | 0.0 | 2.482 |
1 | 3 | 3 | 4 | 36.175 | 0.4 | 2.481 |
-2 | 3 | 4 | 4 | 36.781 | 0.0 | 2.442 |
Atom | x | y | z | Biso | Occ. | |
---|---|---|---|---|---|---|
Si1 | 0.9846 | 0.2280 | 0.0336 | 1.58 | 1.000 | |
Si2 | 0.7832 | 0.5997 | 0.0394 | 1.58 | 1.000 | |
Si3 | 0.0737 | 0.4214 | 0.1796 | 1.58 | 1.000 | |
Si4 | 0.5916 | 0.3665 | 0.9271 | 1.58 | 1.000 | |
Si5 | 0.5000 | 0.5432 | 0.2500 | 1.58 | 0.500 | |
O1 | 0.0446 | 0.3000 | 0.1219 | 2.02 | 1.000 | |
O2 | 0.7505 | 0.2582 | 0.9729 | 2.02 | 1.000 | |
O3 | 0.6865 | 0.4986 | 0.9658 | 2.02 | 1.000 | |
O4 | 0.9467 | 0.5349 | 0.1226 | 2.02 | 1.000 | |
O5 | 0.3069 | 0.4565 | 0.2239 | 2.02 | 1.000 | |
O6 | 0.0000 | 0.3884 | 0.2500 | 2.02 | 0.500 | |
O7 | 0.0248 | 0.0828 | 0.0491 | 0.08 | 1.000 | |
O8 | 0.1145 | 0.2895 | 0.9889 | 2.02 | 1.000 | |
O9 | 0.3922 | 0.3437 | 0.9403 | 2.02 | 1.000 | |
O10 | 0.5271 | 0.3677 | 0.8279 | 2.02 | 1.000 | |
N1 | 0.0000 | 0.9179 | 0.2500 | 23.00 | 0.500 | |
C1 | 0.1421 | 0.0138 | 0.3076 | 17.26 | 1.298 | |
C2 | 0.3424 | 0.0503 | 0.3131 | 17.26 | 1.298 | |
C3 | 0.4940 | 0.1008 | 0.3977 | 17.26 | 1.298 | |
C4 | -0.0791 | 0.8372 | 0.3007 | 17.26 | 1.298 |
User Cell Range (natural numbers 1-5):