Synthesis
Mixture | Dehydration of RUB-52 |
SDA | Diethyldimethylammonium |
Temperature | 70.00 °C |
Duration | 2 d |
Conditions | in air |
Reference |
Marler, Li, Wang & Gies (2011): Acta Crystallographica Section A, Volume 67, Issue C, Pages 650. |
Crystal Structure
Structurally nearly identical materials | None |
Crystal chemically related materials | None |
Chemical composition per unit cell | (C6H16N)2 [Si10O20(OH)2] |
Lattice parameters of the 2D cell of the layer |
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Lattice parameters related to the stacking direction |
|
Space group | P-1 |
XRD reflections representing the 2D cell of the layer |
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XRD reflections representing the layer-layer distance |
|
Reference |
Marler, Li, Wang & Gies (2011): Acta Crystallographica Section A, Volume 67, Issue C, Pages 650. |
Properties
Density (calculated) | 1.892 g/cm3 |
Condensation product | amorphous |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
0 | 1 | 0 | 2 | 7.544 | 100.0 | 11.709 |
1 | 0 | 0 | 2 | 10.889 | 9.3 | 8.119 |
1 | 1 | 0 | 2 | 11.064 | 5.1 | 7.991 |
0 | 0 | 1 | 2 | 12.905 | 2.6 | 6.854 |
-1 | 0 | 1 | 2 | 13.626 | 0.4 | 6.493 |
-1 | -1 | 1 | 2 | 13.696 | 0.0 | 6.460 |
0 | -1 | 1 | 2 | 14.900 | 5.4 | 5.941 |
0 | 1 | 1 | 2 | 15.029 | 1.8 | 5.890 |
0 | 2 | 0 | 2 | 15.121 | 0.1 | 5.855 |
1 | -1 | 0 | 2 | 15.145 | 0.2 | 5.845 |
1 | 2 | 0 | 2 | 15.523 | 0.7 | 5.704 |
-1 | 1 | 1 | 2 | 17.286 | 0.2 | 5.126 |
-1 | -2 | 1 | 2 | 17.453 | 8.1 | 5.077 |
1 | 0 | 1 | 2 | 19.675 | 2.5 | 4.508 |
-2 | -1 | 1 | 2 | 19.823 | 0.2 | 4.475 |
. | . | . | . | . | . | |
1 | 1 | 1 | 2 | 19.823 | 1.7 | 4.475 |
0 | -2 | 1 | 2 | 19.830 | 4.4 | 4.474 |
0 | 2 | 1 | 2 | 20.026 | 13.9 | 4.430 |
2 | 1 | 0 | 2 | 20.695 | 3.8 | 4.288 |
-2 | 0 | 1 | 2 | 21.099 | 3.5 | 4.207 |
1 | -2 | 0 | 2 | 21.373 | 9.1 | 4.154 |
-2 | -2 | 1 | 2 | 21.374 | 0.3 | 4.154 |
1 | 3 | 0 | 2 | 21.826 | 2.8 | 4.069 |
2 | 0 | 0 | 2 | 21.878 | 6.0 | 4.059 |
2 | 2 | 0 | 2 | 22.233 | 5.2 | 3.995 |
1 | -1 | 1 | 2 | 22.305 | 1.6 | 3.983 |
1 | 2 | 1 | 2 | 22.697 | 5.6 | 3.915 |
0 | 3 | 0 | 2 | 22.765 | 1.1 | 3.903 |
-1 | 2 | 1 | 2 | 23.001 | 5.4 | 3.864 |
-1 | -3 | 1 | 2 | 23.212 | 2.3 | 3.829 |
-1 | -1 | 2 | 2 | 24.329 | 11.4 | 3.656 |
-1 | 0 | 2 | 2 | 24.329 | 0.3 | 3.656 |
-2 | 1 | 1 | 2 | 24.788 | 1.5 | 3.589 |
-2 | -3 | 1 | 2 | 25.260 | 3.6 | 3.523 |
2 | -1 | 0 | 2 | 25.421 | 11.0 | 3.501 |
0 | 0 | 2 | 2 | 25.978 | 4.5 | 3.427 |
2 | 3 | 0 | 2 | 26.035 | 7.9 | 3.420 |
0 | -3 | 1 | 2 | 26.140 | 1.0 | 3.406 |
0 | 3 | 1 | 2 | 26.367 | 2.3 | 3.377 |
-2 | -1 | 2 | 2 | 26.428 | 3.1 | 3.370 |
-1 | -2 | 2 | 2 | 26.634 | 7.5 | 3.344 |
-1 | 1 | 2 | 2 | 26.635 | 6.7 | 3.344 |
1 | -2 | 1 | 2 | 26.946 | 2.4 | 3.306 |
0 | -1 | 2 | 2 | 27.015 | 1.6 | 3.298 |
0 | 1 | 2 | 2 | 27.162 | 1.3 | 3.280 |
-2 | 0 | 2 | 2 | 27.449 | 0.6 | 3.247 |
1 | 3 | 1 | 2 | 27.493 | 3.4 | 3.242 |
-2 | -2 | 2 | 2 | 27.593 | 2.6 | 3.230 |
1 | -3 | 0 | 2 | 28.373 | 2.1 | 3.143 |
2 | 1 | 1 | 2 | 28.396 | 0.5 | 3.141 |
1 | 4 | 0 | 2 | 28.859 | 3.0 | 3.091 |
-3 | -1 | 1 | 2 | 29.083 | 0.5 | 3.068 |
2 | 0 | 1 | 2 | 29.252 | 2.6 | 3.051 |
-3 | -2 | 1 | 2 | 29.254 | 2.5 | 3.050 |
2 | 2 | 1 | 2 | 29.591 | 0.5 | 3.016 |
-1 | 3 | 1 | 2 | 29.674 | 3.4 | 3.008 |
-1 | -4 | 1 | 2 | 29.907 | 0.1 | 2.985 |
0 | -2 | 2 | 2 | 30.059 | 0.0 | 2.970 |
-2 | 2 | 1 | 2 | 30.065 | 0.0 | 2.970 |
0 | 2 | 2 | 2 | 30.326 | 0.2 | 2.945 |
-2 | 1 | 2 | 2 | 30.455 | 0.4 | 2.933 |
0 | 4 | 0 | 2 | 30.513 | 0.1 | 2.927 |
2 | -2 | 0 | 2 | 30.564 | 0.6 | 2.923 |
-2 | -4 | 1 | 2 | 30.657 | 0.1 | 2.914 |
-2 | -3 | 2 | 2 | 30.715 | 0.5 | 2.909 |
-1 | -3 | 2 | 2 | 30.765 | 0.6 | 2.904 |
-1 | 2 | 2 | 2 | 30.767 | 0.1 | 2.904 |
-3 | 0 | 1 | 2 | 30.901 | 0.1 | 2.891 |
2 | 4 | 0 | 2 | 31.341 | 0.0 | 2.852 |
-3 | -3 | 1 | 2 | 31.384 | 4.0 | 2.848 |
3 | 1 | 0 | 2 | 31.403 | 5.3 | 2.846 |
3 | 2 | 0 | 2 | 31.594 | 0.6 | 2.830 |
1 | 0 | 2 | 2 | 31.710 | 0.2 | 2.819 |
1 | 1 | 2 | 2 | 31.837 | 0.0 | 2.809 |
2 | -1 | 1 | 2 | 32.008 | 1.3 | 2.794 |
-3 | -1 | 2 | 2 | 32.458 | 0.1 | 2.756 |
-3 | -2 | 2 | 2 | 32.582 | 0.7 | 2.746 |
2 | 3 | 1 | 2 | 32.632 | 0.2 | 2.742 |
1 | -3 | 1 | 2 | 32.821 | 0.4 | 2.727 |
3 | 0 | 0 | 2 | 33.075 | 0.0 | 2.706 |
0 | -4 | 1 | 2 | 33.131 | 0.1 | 2.702 |
0 | 4 | 1 | 2 | 33.375 | 0.0 | 2.683 |
1 | -1 | 2 | 2 | 33.429 | 0.1 | 2.678 |
1 | 4 | 1 | 2 | 33.461 | 0.0 | 2.676 |
3 | 3 | 0 | 2 | 33.620 | 0.0 | 2.664 |
1 | 2 | 2 | 2 | 33.791 | 0.0 | 2.650 |
-3 | 0 | 2 | 2 | 34.144 | 0.6 | 2.624 |
-3 | 1 | 1 | 2 | 34.423 | 0.0 | 2.603 |
-3 | -3 | 2 | 2 | 34.497 | 0.0 | 2.598 |
0 | -3 | 2 | 2 | 34.632 | 0.0 | 2.588 |
-2 | 2 | 2 | 2 | 34.982 | 0.0 | 2.563 |
0 | 3 | 2 | 2 | 34.984 | 0.1 | 2.563 |
-3 | -4 | 1 | 2 | 35.152 | 0.3 | 2.551 |
-2 | -4 | 2 | 2 | 35.327 | 1.2 | 2.539 |
1 | -4 | 0 | 2 | 35.785 | 0.2 | 2.507 |
-1 | -4 | 2 | 2 | 36.163 | 0.0 | 2.482 |
-1 | 3 | 2 | 2 | 36.165 | 0.0 | 2.482 |
2 | -2 | 1 | 2 | 36.279 | 1.3 | 2.474 |
1 | 5 | 0 | 2 | 36.295 | 0.5 | 2.473 |
-2 | 3 | 1 | 2 | 36.318 | 0.0 | 2.472 |
3 | -1 | 0 | 2 | 36.382 | 0.0 | 2.467 |
2 | -3 | 0 | 2 | 36.713 | 0.0 | 2.446 |
1 | -2 | 2 | 2 | 36.763 | 0.2 | 2.443 |
-1 | -1 | 3 | 2 | 36.840 | 0.0 | 2.438 |
-1 | 0 | 3 | 2 | 36.869 | 0.4 | 2.436 |
-1 | 4 | 1 | 2 | 36.879 | 1.3 | 2.435 |
-2 | -1 | 3 | 2 | 36.896 | 0.2 | 2.434 |
-2 | -5 | 1 | 2 | 36.986 | 0.2 | 2.428 |
Atom | x | y | z | Biso | Occ. | |
---|---|---|---|---|---|---|
Si1 | 0.2261 | 0.4057 | 0.4406 | 2.37 | 1.000 | |
Si2 | 0.8586 | 0.4147 | 0.2605 | 2.37 | 1.000 | |
Si3 | 0.4160 | 0.7330 | 0.3759 | 2.37 | 1.000 | |
Si4 | 0.6622 | 0.4897 | 0.8114 | 2.37 | 1.000 | |
Si5 | 0.6286 | 0.2788 | 0.2304 | 2.37 | 1.000 | |
O1 | 0.2239 | 0.4932 | 0.3003 | 3.01 | 1.000 | |
O2 | 0.3834 | 0.2894 | 0.5178 | 3.01 | 1.000 | |
O3 | 0.0582 | 0.3699 | 0.3310 | 3.01 | 1.000 | |
O4 | 0.7875 | 0.5238 | 0.3710 | 3.01 | 1.000 | |
O5 | 0.3602 | 0.8342 | 0.2526 | 3.01 | 1.000 | |
O6 | 0.4106 | 0.6111 | 0.2863 | 3.01 | 1.000 | |
O7 | 0.5045 | 0.5957 | 0.8052 | 3.01 | 1.000 | |
O8 | 0.7792 | 0.4548 | 0.0307 | 3.01 | 1.000 | |
O9 | 0.7994 | 0.3121 | 0.2898 | 3.01 | 1.000 | |
O10 | 0.6204 | 0.1900 | 0.0676 | 3.01 | 1.000 | |
O11 | 0.6389 | 0.2379 | 0.4315 | 3.01 | 1.000 | |
C1 | 0.7069 | 0.9176 | 0.2422 | 9.48 | 1.196 | |
C2 | 0.9602 | 0.8540 | 0.2204 | 9.48 | 1.196 | |
C3 | 0.8617 | 0.7091 | 0.1638 | 9.48 | 1.345 | |
C4 | 0.7257 | 0.8733 | 0.9249 | 9.48 | 1.345 | |
C5 | 0.7636 | 0.9260 | 0.4681 | 20.45 | 1.345 | |
C6 | 0.9419 | 0.9455 | 0.0948 | 20.45 | 1.345 | |
N1 | 0.7996 | 0.8335 | 0.1322 | 9.48 | 0.897 |
No 3D representation available
No data available