Synthesis
Mixture | 1 SiO2 : 1.0-1.5 SDA : 12-18 H2O |
SDA | Diethyldimethylammonium |
Temperature | 150.00 °C |
Duration | 7-15 d |
Conditions | n/a |
Reference |
Marler, Li, Wang & Gies (2011): Acta Crystallographica Section A, Volume 67, Issue C, Pages 650. |
Crystal Structure
Structurally nearly identical materials | None |
Crystal chemically related materials | None |
Chemical composition per unit cell | (C6H16N)2 [Si10O20(OH)2] ∙ 6 H2O |
Lattice parameters of the 2D cell of the layer |
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Lattice parameters related to the stacking direction |
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Space group | P-1 |
XRD reflections representing the 2D cell of the layer |
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XRD reflections representing the layer-layer distance |
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Reference |
Marler, Li, Wang & Gies (2011): Acta Crystallographica Section A, Volume 67, Issue C, Pages 650. |
Properties
Density (calculated) | 1.624 g/cm3 |
Condensation product | amorphous |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
1 | 0 | 0 | 2 | 5.794 | 100.0 | 15.241 |
0 | 1 | 0 | 2 | 10.561 | 5.1 | 8.370 |
1 | -1 | 0 | 2 | 10.938 | 2.2 | 8.082 |
2 | 0 | 0 | 2 | 11.603 | 1.7 | 7.620 |
1 | 1 | 0 | 2 | 13.076 | 0.1 | 6.765 |
0 | -1 | 1 | 2 | 13.144 | 1.6 | 6.730 |
-1 | -1 | 1 | 2 | 13.432 | 0.3 | 6.587 |
-1 | 0 | 1 | 2 | 13.545 | 0.6 | 6.532 |
2 | -1 | 0 | 2 | 13.979 | 0.0 | 6.330 |
0 | 0 | 1 | 2 | 14.197 | 0.1 | 6.233 |
1 | -1 | 1 | 2 | 15.261 | 0.3 | 5.801 |
-2 | 0 | 1 | 2 | 15.270 | 1.2 | 5.798 |
-2 | -1 | 1 | 2 | 15.997 | 3.8 | 5.536 |
1 | 0 | 1 | 2 | 16.959 | 0.0 | 5.224 |
2 | 1 | 0 | 2 | 17.280 | 0.9 | 5.128 |
. | . | . | . | . | . | |
3 | 0 | 0 | 2 | 17.442 | 0.4 | 5.080 |
3 | -1 | 0 | 2 | 18.428 | 2.5 | 4.811 |
-3 | 0 | 1 | 2 | 18.740 | 3.7 | 4.731 |
2 | -1 | 1 | 2 | 19.012 | 3.0 | 4.664 |
0 | -2 | 1 | 2 | 19.220 | 0.5 | 4.614 |
-3 | -1 | 1 | 2 | 20.001 | 0.7 | 4.436 |
-1 | -2 | 1 | 2 | 20.077 | 0.7 | 4.419 |
1 | -2 | 1 | 2 | 20.102 | 0.9 | 4.414 |
-1 | 1 | 1 | 2 | 20.307 | 0.1 | 4.370 |
1 | -2 | 0 | 2 | 20.789 | 1.8 | 4.269 |
-2 | 1 | 1 | 2 | 20.895 | 0.6 | 4.248 |
2 | 0 | 1 | 2 | 21.037 | 2.6 | 4.220 |
0 | 2 | 0 | 2 | 21.213 | 0.1 | 4.185 |
0 | 1 | 1 | 2 | 21.372 | 2.0 | 4.154 |
2 | -2 | 0 | 2 | 21.978 | 2.1 | 4.041 |
3 | 1 | 0 | 2 | 22.266 | 2.7 | 3.989 |
-2 | -2 | 1 | 2 | 22.485 | 0.9 | 3.951 |
2 | -2 | 1 | 2 | 22.530 | 1.8 | 3.943 |
-3 | 1 | 1 | 2 | 23.014 | 1.3 | 3.861 |
1 | 2 | 0 | 2 | 23.166 | 5.3 | 3.836 |
-4 | 0 | 1 | 2 | 23.211 | 0.4 | 3.829 |
4 | 0 | 0 | 2 | 23.327 | 0.0 | 3.810 |
4 | -1 | 0 | 2 | 23.531 | 0.1 | 3.778 |
3 | -1 | 1 | 2 | 23.659 | 3.6 | 3.758 |
1 | 1 | 1 | 2 | 23.878 | 0.4 | 3.724 |
-1 | -1 | 2 | 2 | 24.475 | 0.3 | 3.634 |
3 | -2 | 0 | 2 | 24.557 | 1.1 | 3.622 |
-4 | -1 | 1 | 2 | 24.786 | 0.5 | 3.589 |
-2 | -1 | 2 | 2 | 24.960 | 3.1 | 3.565 |
0 | -1 | 2 | 2 | 25.384 | 1.4 | 3.506 |
3 | 0 | 1 | 2 | 25.846 | 0.3 | 3.444 |
-3 | -2 | 1 | 2 | 26.037 | 0.3 | 3.419 |
3 | -2 | 1 | 2 | 26.096 | 0.6 | 3.412 |
-1 | -2 | 2 | 2 | 26.103 | 1.7 | 3.411 |
-4 | 1 | 1 | 2 | 26.316 | 1.6 | 3.384 |
2 | 2 | 0 | 2 | 26.326 | 2.4 | 3.383 |
0 | -2 | 2 | 2 | 26.466 | 0.5 | 3.365 |
-3 | -1 | 2 | 2 | 26.766 | 0.9 | 3.328 |
-2 | -2 | 2 | 2 | 27.053 | 0.7 | 3.293 |
-2 | 0 | 2 | 2 | 27.284 | 2.7 | 3.266 |
-1 | 0 | 2 | 2 | 27.328 | 0.9 | 3.261 |
2 | 1 | 1 | 2 | 27.456 | 0.1 | 3.246 |
1 | -1 | 2 | 2 | 27.557 | 1.1 | 3.234 |
4 | 1 | 0 | 2 | 27.651 | 0.5 | 3.224 |
1 | -2 | 2 | 2 | 28.093 | 0.1 | 3.174 |
4 | -2 | 0 | 2 | 28.171 | 0.8 | 3.165 |
-5 | 0 | 1 | 2 | 28.246 | 0.3 | 3.157 |
0 | -3 | 1 | 2 | 28.255 | 0.5 | 3.156 |
1 | -3 | 1 | 2 | 28.413 | 0.1 | 3.139 |
-3 | 0 | 2 | 2 | 28.494 | 0.1 | 3.130 |
0 | 0 | 2 | 2 | 28.618 | 0.0 | 3.117 |
4 | -1 | 1 | 2 | 28.809 | 0.0 | 3.097 |
5 | -1 | 0 | 2 | 28.986 | 0.7 | 3.078 |
-3 | -2 | 2 | 2 | 29.196 | 0.1 | 3.056 |
5 | 0 | 0 | 2 | 29.276 | 0.4 | 3.048 |
-1 | -3 | 1 | 2 | 29.316 | 1.2 | 3.044 |
-2 | 2 | 1 | 2 | 29.554 | 0.3 | 3.020 |
-1 | 2 | 1 | 2 | 29.585 | 0.1 | 3.017 |
-4 | -1 | 2 | 2 | 29.671 | 0.8 | 3.008 |
2 | -3 | 1 | 2 | 29.770 | 0.5 | 2.999 |
-5 | -1 | 1 | 2 | 30.019 | 0.1 | 2.974 |
3 | 2 | 0 | 2 | 30.348 | 0.3 | 2.943 |
-4 | -2 | 1 | 2 | 30.365 | 0.6 | 2.941 |
4 | -2 | 1 | 2 | 30.433 | 0.4 | 2.935 |
-5 | 1 | 1 | 2 | 30.447 | 0.7 | 2.934 |
-3 | 2 | 1 | 2 | 30.689 | 0.4 | 2.911 |
2 | -1 | 2 | 2 | 30.747 | 0.3 | 2.906 |
0 | 2 | 1 | 2 | 30.781 | 0.1 | 2.902 |
2 | -2 | 2 | 2 | 30.802 | 0.1 | 2.901 |
-4 | 0 | 2 | 2 | 30.820 | 0.1 | 2.899 |
1 | 0 | 2 | 2 | 31.013 | 0.0 | 2.881 |
4 | 0 | 1 | 2 | 31.089 | 1.8 | 2.874 |
1 | -3 | 0 | 2 | 31.342 | 2.7 | 2.852 |
0 | -3 | 2 | 2 | 31.453 | 0.2 | 2.842 |
-2 | -3 | 1 | 2 | 31.482 | 0.8 | 2.839 |
-1 | -3 | 2 | 2 | 31.571 | 0.2 | 2.832 |
2 | -3 | 0 | 2 | 31.746 | 0.4 | 2.816 |
3 | 1 | 1 | 2 | 31.777 | 0.0 | 2.814 |
0 | 3 | 0 | 2 | 32.055 | 0.1 | 2.790 |
3 | -3 | 1 | 2 | 32.190 | 0.2 | 2.779 |
-4 | -2 | 2 | 2 | 32.317 | 0.0 | 2.768 |
1 | -3 | 2 | 2 | 32.443 | 0.0 | 2.757 |
5 | -2 | 0 | 2 | 32.507 | 0.0 | 2.752 |
-2 | -3 | 2 | 2 | 32.786 | 0.0 | 2.729 |
-4 | 2 | 1 | 2 | 32.883 | 0.4 | 2.722 |
1 | 2 | 1 | 2 | 33.026 | 0.0 | 2.710 |
-2 | 1 | 2 | 2 | 33.176 | 0.4 | 2.698 |
3 | -3 | 0 | 2 | 33.229 | 0.0 | 2.694 |
5 | 1 | 0 | 2 | 33.287 | 0.2 | 2.689 |
-5 | -1 | 2 | 2 | 33.416 | 0.1 | 2.679 |
-1 | 1 | 2 | 2 | 33.616 | 0.1 | 2.664 |
-6 | 0 | 1 | 2 | 33.638 | 0.0 | 2.662 |
-3 | 1 | 2 | 2 | 33.798 | 0.2 | 2.650 |
1 | 3 | 0 | 2 | 33.820 | 0.0 | 2.648 |
-5 | 0 | 2 | 2 | 34.057 | 0.8 | 2.630 |
5 | -1 | 1 | 2 | 34.280 | 0.1 | 2.614 |
2 | 0 | 2 | 2 | 34.305 | 0.0 | 2.612 |
3 | -2 | 2 | 2 | 34.362 | 0.0 | 2.608 |
2 | -3 | 2 | 2 | 34.455 | 0.5 | 2.601 |
-3 | -3 | 1 | 2 | 34.568 | 0.8 | 2.593 |
6 | -1 | 0 | 2 | 34.672 | 0.2 | 2.585 |
3 | -1 | 2 | 2 | 34.705 | 0.1 | 2.583 |
4 | 2 | 0 | 2 | 34.970 | 0.0 | 2.564 |
-3 | -3 | 2 | 2 | 34.997 | 0.0 | 2.562 |
0 | 1 | 2 | 2 | 35.083 | 0.0 | 2.556 |
Atom | x | y | z | Biso | Occ. | |
---|---|---|---|---|---|---|
Si1 | -0.0119 | 0.3455 | 0.1415 | 1.27 | 1.000 | |
Si2 | 0.9447 | 0.1525 | 0.3623 | 1.27 | 1.000 | |
Si3 | 0.1803 | 0.5343 | 0.9867 | 1.27 | 1.000 | |
Si4 | 0.0690 | 0.2024 | 0.7807 | 1.27 | 1.000 | |
Si5 | 0.1656 | 0.6030 | 0.4254 | 1.27 | 1.000 | |
O1 | 0.9038 | 0.4191 | 0.1230 | 1.73 | 1.000 | |
O2 | 0.0710 | 0.4873 | 0.3094 | 1.73 | 1.000 | |
O3 | 0.9809 | 0.2147 | 0.2212 | 1.73 | 1.000 | |
O4 | 0.8720 | 0.2331 | 0.4645 | 1.73 | 1.000 | |
O5 | 0.1575 | 0.3366 | 0.8893 | 1.73 | 1.000 | |
O6 | 0.2562 | 0.5957 | 0.9191 | 1.73 | 1.000 | |
O7 | 0.9945 | 0.2581 | 0.8951 | 1.73 | 1.000 | |
O8 | 0.0910 | 0.0397 | 0.7750 | 1.73 | 1.000 | |
O9 | 0.0323 | 0.1858 | 0.5458 | 1.73 | 1.000 | |
O10 | 0.2517 | 0.5988 | 0.5870 | 1.73 | 1.000 | |
O11 | 0.1995 | 0.6143 | 0.2405 | 1.73 | 1.000 | |
N1 | 0.6844 | 0.9408 | 0.6758 | 22.90 | 1.000 | |
C1 | 0.6673 | 0.7648 | 0.6152 | 22.90 | 1.333 | |
C2 | 0.7735 | 0.9470 | 0.6376 | 22.90 | 1.333 | |
C3 | 0.6278 | -0.0071 | 0.5212 | 22.90 | 1.500 | |
C4 | 0.6664 | 0.9896 | 0.8837 | 22.90 | 1.500 | |
C5 | 0.6685 | 0.7179 | 0.3785 | 78.45 | 1.500 | |
C6 | 0.8150 | 0.8966 | 0.8061 | 78.45 | 1.500 | |
W1 | 0.3969 | 0.6752 | 0.5575 | 11.52 | 1.250 | |
W2 | 0.4190 | 0.6335 | 0.1310 | 11.52 | 1.250 | |
W3 | 0.5148 | 0.6635 | 0.8661 | 11.52 | 1.250 |
No 3D representation available
No data available