Synthesis
Mixture | 1 SiO2 : 1 SDA : 10 H2O |
SDA | Di-4,1-(N-methylpiperidinium)butane |
Temperature | 120.00 °C |
Duration | 4 d |
Conditions | n/a |
Reference |
Zhang, Grünewald-Lüke, Marler, Wei & Gies (2012): Book of Abstracts IV Int. Workshop on Layered Materials, Volume None, Issue , Pages 139-140. |
Crystal Structure
Structurally nearly identical materials | None |
Crystal chemically related materials | None |
Chemical composition per unit cell | (C16H34N2)4 [Si32O64(OH)8] ∙ 28 H2O |
Lattice parameters of the 2D cell of the layer |
|
Lattice parameters related to the stacking direction |
|
Space group | C2/c |
XRD reflections representing the 2D cell of the layer |
|
XRD reflections representing the layer-layer distance |
|
Reference |
(): , Volume , Issue , Pages . |
Properties
Density (calculated) | 1.615 g/cm3 |
Condensation product | amorphous |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
0 | 0 | 1 | 2 | 5.088 | 100.0 | 17.356 |
0 | 1 | 0 | 2 | 8.684 | 4.5 | 10.175 |
1 | 0 | 0 | 2 | 8.684 | 1.3 | 10.175 |
-1 | 0 | 1 | 2 | 9.756 | 9.8 | 9.059 |
0 | -1 | 1 | 2 | 9.756 | 1.0 | 9.059 |
0 | 0 | 2 | 2 | 10.185 | 0.2 | 8.678 |
0 | 1 | 1 | 2 | 10.373 | 0.2 | 8.521 |
1 | 0 | 1 | 2 | 10.373 | 0.4 | 8.521 |
1 | 1 | 0 | 2 | 10.959 | 0.2 | 8.067 |
-1 | -1 | 1 | 2 | 11.563 | 0.2 | 7.647 |
1 | 1 | 1 | 2 | 12.594 | 1.2 | 7.023 |
-1 | 0 | 2 | 2 | 12.926 | 1.5 | 6.843 |
0 | -1 | 2 | 2 | 12.926 | 0.1 | 6.843 |
1 | -1 | 0 | 2 | 13.497 | 0.4 | 6.555 |
0 | 1 | 2 | 2 | 13.857 | 0.3 | 6.386 |
. | . | . | . | . | . | |
1 | 0 | 2 | 2 | 13.857 | 0.7 | 6.386 |
-1 | -1 | 2 | 2 | 14.124 | 0.4 | 6.265 |
-1 | 1 | 1 | 2 | 14.432 | 1.3 | 6.132 |
1 | -1 | 1 | 2 | 14.432 | 1.1 | 6.132 |
0 | 0 | 3 | 2 | 15.303 | 3.9 | 5.785 |
1 | 1 | 2 | 2 | 15.796 | 0.1 | 5.606 |
-1 | 1 | 2 | 2 | 16.937 | 1.7 | 5.231 |
1 | -1 | 2 | 2 | 16.937 | 1.4 | 5.231 |
-1 | 0 | 3 | 2 | 17.078 | 0.8 | 5.188 |
0 | -1 | 3 | 2 | 17.078 | 0.6 | 5.188 |
0 | 2 | 0 | 2 | 17.418 | 3.8 | 5.087 |
2 | 0 | 0 | 2 | 17.418 | 1.3 | 5.087 |
-2 | 0 | 1 | 2 | 17.807 | 0.9 | 4.977 |
0 | -2 | 1 | 2 | 17.807 | 0.6 | 4.977 |
1 | 2 | 0 | 2 | 17.813 | 0.7 | 4.976 |
2 | 1 | 0 | 2 | 17.813 | 0.8 | 4.976 |
-1 | -1 | 3 | 2 | 17.833 | 1.2 | 4.970 |
-2 | -1 | 1 | 2 | 18.020 | 2.4 | 4.919 |
-1 | -2 | 1 | 2 | 18.020 | 1.7 | 4.919 |
0 | 1 | 3 | 2 | 18.148 | 1.2 | 4.884 |
1 | 0 | 3 | 2 | 18.148 | 1.3 | 4.884 |
0 | 2 | 1 | 2 | 18.500 | 1.9 | 4.792 |
2 | 0 | 1 | 2 | 18.500 | 2.1 | 4.792 |
1 | 2 | 1 | 2 | 19.039 | 0.0 | 4.658 |
2 | 1 | 1 | 2 | 19.039 | 0.0 | 4.658 |
-2 | 0 | 2 | 2 | 19.584 | 0.0 | 4.529 |
0 | -2 | 2 | 2 | 19.584 | 0.1 | 4.529 |
-2 | -1 | 2 | 2 | 19.618 | 0.1 | 4.521 |
-1 | -2 | 2 | 2 | 19.618 | 0.2 | 4.521 |
1 | 1 | 3 | 2 | 19.838 | 0.0 | 4.472 |
0 | 0 | 4 | 2 | 20.452 | 1.6 | 4.339 |
-1 | 1 | 3 | 2 | 20.458 | 1.7 | 4.338 |
1 | -1 | 3 | 2 | 20.458 | 1.7 | 4.338 |
0 | 2 | 2 | 2 | 20.833 | 0.9 | 4.261 |
2 | 0 | 2 | 2 | 20.833 | 1.4 | 4.261 |
1 | -2 | 0 | 2 | 21.044 | 2.5 | 4.218 |
2 | -1 | 0 | 2 | 21.044 | 2.4 | 4.218 |
1 | 2 | 2 | 2 | 21.463 | 2.8 | 4.137 |
2 | 1 | 2 | 2 | 21.463 | 2.7 | 4.137 |
-2 | 1 | 1 | 2 | 21.517 | 2.4 | 4.126 |
1 | -2 | 1 | 2 | 21.517 | 2.6 | 4.126 |
-1 | 0 | 4 | 2 | 21.679 | 0.3 | 4.096 |
0 | -1 | 4 | 2 | 21.679 | 0.2 | 4.096 |
-1 | 2 | 1 | 2 | 21.810 | 0.1 | 4.072 |
2 | -1 | 1 | 2 | 21.810 | 0.2 | 4.072 |
2 | 2 | 0 | 2 | 22.020 | 3.2 | 4.033 |
-2 | -2 | 1 | 2 | 22.047 | 4.1 | 4.029 |
-1 | -1 | 4 | 2 | 22.141 | 4.9 | 4.012 |
-2 | -1 | 3 | 2 | 22.320 | 1.7 | 3.980 |
-1 | -2 | 3 | 2 | 22.320 | 2.3 | 3.980 |
-2 | 0 | 3 | 2 | 22.431 | 0.3 | 3.960 |
0 | -2 | 3 | 2 | 22.431 | 0.2 | 3.960 |
0 | 1 | 4 | 2 | 22.819 | 0.0 | 3.894 |
1 | 0 | 4 | 2 | 22.819 | 0.0 | 3.894 |
-2 | 1 | 2 | 2 | 23.157 | 1.1 | 3.838 |
1 | -2 | 2 | 2 | 23.157 | 0.9 | 3.838 |
2 | 2 | 1 | 2 | 23.169 | 1.2 | 3.836 |
-2 | -2 | 2 | 2 | 23.245 | 2.6 | 3.823 |
-1 | 2 | 2 | 2 | 23.700 | 1.5 | 3.751 |
2 | -1 | 2 | 2 | 23.700 | 1.6 | 3.751 |
0 | 2 | 3 | 2 | 24.071 | 0.0 | 3.694 |
2 | 0 | 3 | 2 | 24.071 | 0.0 | 3.694 |
1 | 1 | 4 | 2 | 24.329 | 0.6 | 3.656 |
-1 | 1 | 4 | 2 | 24.584 | 0.9 | 3.618 |
1 | -1 | 4 | 2 | 24.584 | 0.9 | 3.618 |
1 | 2 | 3 | 2 | 24.751 | 0.1 | 3.594 |
2 | 1 | 3 | 2 | 24.751 | 0.1 | 3.594 |
2 | 2 | 2 | 2 | 25.343 | 0.4 | 3.512 |
-2 | -2 | 3 | 2 | 25.459 | 0.4 | 3.496 |
0 | 0 | 5 | 2 | 25.643 | 0.0 | 3.471 |
-2 | 1 | 3 | 2 | 25.754 | 0.0 | 3.457 |
1 | -2 | 3 | 2 | 25.754 | 0.0 | 3.457 |
-2 | -1 | 4 | 2 | 25.799 | 0.0 | 3.450 |
-1 | -2 | 4 | 2 | 25.799 | 0.0 | 3.450 |
1 | 3 | 0 | 2 | 25.916 | 0.0 | 3.435 |
3 | 1 | 0 | 2 | 25.916 | 0.0 | 3.435 |
-3 | -1 | 1 | 2 | 25.939 | 0.0 | 3.432 |
-1 | -3 | 1 | 2 | 25.939 | 0.0 | 3.432 |
-2 | 0 | 4 | 2 | 26.020 | 0.0 | 3.422 |
0 | -2 | 4 | 2 | 26.020 | 0.0 | 3.422 |
0 | 3 | 0 | 2 | 26.256 | 1.2 | 3.392 |
3 | 0 | 0 | 2 | 26.256 | 0.3 | 3.392 |
-3 | 0 | 1 | 2 | 26.400 | 0.0 | 3.373 |
0 | -3 | 1 | 2 | 26.400 | 0.0 | 3.373 |
-1 | 2 | 3 | 2 | 26.489 | 0.0 | 3.362 |
2 | -1 | 3 | 2 | 26.489 | 0.0 | 3.362 |
-1 | 0 | 5 | 2 | 26.523 | 0.0 | 3.358 |
0 | -1 | 5 | 2 | 26.523 | 0.0 | 3.358 |
-1 | -1 | 5 | 2 | 26.787 | 0.0 | 3.325 |
1 | 3 | 1 | 2 | 26.908 | 0.0 | 3.311 |
3 | 1 | 1 | 2 | 26.908 | 0.0 | 3.311 |
-3 | -1 | 2 | 2 | 26.975 | 0.1 | 3.303 |
-1 | -3 | 2 | 2 | 26.975 | 0.0 | 3.303 |
0 | 3 | 1 | 2 | 27.118 | 0.9 | 3.286 |
3 | 0 | 1 | 2 | 27.118 | 0.6 | 3.286 |
2 | -2 | 0 | 2 | 27.185 | 1.2 | 3.278 |
-3 | 0 | 2 | 2 | 27.536 | 0.4 | 3.237 |
0 | -3 | 2 | 2 | 27.536 | 0.2 | 3.237 |
-2 | 2 | 1 | 2 | 27.675 | 0.4 | 3.221 |
2 | -2 | 1 | 2 | 27.675 | 0.4 | 3.221 |
0 | 1 | 5 | 2 | 27.707 | 0.4 | 3.217 |
1 | 0 | 5 | 2 | 27.707 | 0.4 | 3.217 |
0 | 2 | 4 | 2 | 27.922 | 0.1 | 3.193 |
2 | 0 | 4 | 2 | 27.922 | 0.1 | 3.193 |
2 | 2 | 3 | 2 | 28.321 | 0.2 | 3.149 |
-3 | -2 | 1 | 2 | 28.372 | 0.3 | 3.143 |
-2 | -3 | 1 | 2 | 28.372 | 0.3 | 3.143 |
2 | 3 | 0 | 2 | 28.464 | 0.2 | 3.133 |
3 | 2 | 0 | 2 | 28.464 | 0.3 | 3.133 |
-2 | -2 | 4 | 2 | 28.469 | 0.2 | 3.133 |
1 | 2 | 4 | 2 | 28.630 | 0.1 | 3.115 |
2 | 1 | 4 | 2 | 28.630 | 0.2 | 3.115 |
1 | 3 | 2 | 2 | 28.819 | 0.2 | 3.095 |
3 | 1 | 2 | 2 | 28.819 | 0.3 | 3.095 |
0 | 3 | 2 | 2 | 28.905 | 0.2 | 3.086 |
3 | 0 | 2 | 2 | 28.905 | 0.4 | 3.086 |
-3 | -1 | 3 | 2 | 28.923 | 0.4 | 3.085 |
-1 | -3 | 3 | 2 | 28.923 | 0.2 | 3.085 |
-2 | 1 | 4 | 2 | 29.069 | 0.6 | 3.069 |
1 | -2 | 4 | 2 | 29.069 | 0.4 | 3.069 |
-1 | 1 | 5 | 2 | 29.086 | 0.6 | 3.068 |
1 | -1 | 5 | 2 | 29.086 | 0.5 | 3.068 |
1 | 1 | 5 | 2 | 29.090 | 0.6 | 3.067 |
-2 | 2 | 2 | 2 | 29.100 | 0.6 | 3.066 |
2 | -2 | 2 | 2 | 29.100 | 0.5 | 3.066 |
-3 | -2 | 2 | 2 | 29.218 | 1.0 | 3.054 |
-2 | -3 | 2 | 2 | 29.218 | 0.9 | 3.054 |
1 | -3 | 0 | 2 | 29.390 | 1.0 | 3.037 |
3 | -1 | 0 | 2 | 29.390 | 1.1 | 3.037 |
2 | 3 | 1 | 2 | 29.487 | 0.7 | 3.027 |
3 | 2 | 1 | 2 | 29.487 | 0.8 | 3.027 |
-3 | 0 | 3 | 2 | 29.559 | 0.8 | 3.020 |
0 | -3 | 3 | 2 | 29.559 | 0.5 | 3.020 |
-3 | 1 | 1 | 2 | 29.629 | 0.6 | 3.013 |
1 | -3 | 1 | 2 | 29.629 | 0.3 | 3.013 |
-2 | -1 | 5 | 2 | 29.809 | 0.3 | 2.995 |
-1 | -2 | 5 | 2 | 29.809 | 0.2 | 2.995 |
-1 | 2 | 4 | 2 | 29.945 | 0.3 | 2.982 |
2 | -1 | 4 | 2 | 29.945 | 0.2 | 2.982 |
-1 | 3 | 1 | 2 | 30.063 | 0.2 | 2.970 |
3 | -1 | 1 | 2 | 30.063 | 0.3 | 2.970 |
-2 | 0 | 5 | 2 | 30.110 | 0.2 | 2.966 |
0 | -2 | 5 | 2 | 30.110 | 0.2 | 2.966 |
-3 | 1 | 2 | 2 | 30.761 | 0.4 | 2.904 |
1 | -3 | 2 | 2 | 30.761 | 0.2 | 2.904 |
0 | 0 | 6 | 2 | 30.888 | 1.3 | 2.893 |
-3 | -2 | 3 | 2 | 30.932 | 1.6 | 2.889 |
-2 | -3 | 3 | 2 | 30.932 | 1.7 | 2.889 |
-2 | 2 | 3 | 2 | 31.342 | 1.0 | 2.852 |
2 | -2 | 3 | 2 | 31.342 | 0.9 | 2.852 |
2 | 3 | 2 | 2 | 31.357 | 0.7 | 2.850 |
3 | 2 | 2 | 2 | 31.357 | 0.8 | 2.850 |
0 | 3 | 3 | 2 | 31.471 | 0.2 | 2.840 |
3 | 0 | 3 | 2 | 31.471 | 0.4 | 2.840 |
1 | 3 | 3 | 2 | 31.495 | 0.2 | 2.838 |
3 | 1 | 3 | 2 | 31.495 | 0.3 | 2.838 |
-1 | 0 | 6 | 2 | 31.531 | 0.2 | 2.835 |
0 | -1 | 6 | 2 | 31.531 | 0.2 | 2.835 |
-1 | 3 | 2 | 2 | 31.595 | 0.1 | 2.830 |
3 | -1 | 2 | 2 | 31.595 | 0.3 | 2.830 |
-3 | -1 | 4 | 2 | 31.629 | 0.3 | 2.827 |
-1 | -3 | 4 | 2 | 31.629 | 0.1 | 2.827 |
-1 | -1 | 6 | 2 | 31.654 | 0.2 | 2.824 |
2 | 2 | 4 | 2 | 31.902 | 1.0 | 2.803 |
-2 | -2 | 5 | 2 | 32.072 | 0.7 | 2.789 |
0 | 2 | 5 | 2 | 32.195 | 0.3 | 2.778 |
2 | 0 | 5 | 2 | 32.195 | 0.4 | 2.778 |
-3 | 0 | 4 | 2 | 32.318 | 0.2 | 2.768 |
0 | -3 | 4 | 2 | 32.318 | 0.1 | 2.768 |
-3 | 1 | 3 | 2 | 32.702 | 0.1 | 2.736 |
1 | -3 | 3 | 2 | 32.702 | 0.1 | 2.736 |
0 | 1 | 6 | 2 | 32.748 | 0.1 | 2.733 |
1 | 0 | 6 | 2 | 32.748 | 0.1 | 2.733 |
-2 | 1 | 5 | 2 | 32.911 | 0.1 | 2.719 |
1 | -2 | 5 | 2 | 32.911 | 0.1 | 2.719 |
1 | 2 | 5 | 2 | 32.918 | 0.1 | 2.719 |
2 | 1 | 5 | 2 | 32.918 | 0.1 | 2.719 |
-3 | -3 | 1 | 2 | 33.115 | 0.2 | 2.703 |
3 | 3 | 0 | 2 | 33.294 | 0.1 | 2.689 |
-3 | -2 | 4 | 2 | 33.394 | 0.1 | 2.681 |
-2 | -3 | 4 | 2 | 33.394 | 0.1 | 2.681 |
-3 | -3 | 2 | 2 | 33.757 | 0.1 | 2.653 |
-1 | 1 | 6 | 2 | 33.844 | 0.1 | 2.646 |
1 | -1 | 6 | 2 | 33.844 | 0.1 | 2.646 |
-1 | 3 | 3 | 2 | 33.881 | 0.1 | 2.644 |
3 | -1 | 3 | 2 | 33.881 | 0.1 | 2.644 |
-1 | 2 | 5 | 2 | 33.890 | 0.1 | 2.643 |
2 | -1 | 5 | 2 | 33.890 | 0.1 | 2.643 |
2 | 3 | 3 | 2 | 33.949 | 0.1 | 2.639 |
3 | 2 | 3 | 2 | 33.949 | 0.1 | 2.639 |
1 | 1 | 6 | 2 | 34.041 | 0.2 | 2.632 |
-2 | -1 | 6 | 2 | 34.190 | 0.4 | 2.620 |
-1 | -2 | 6 | 2 | 34.190 | 0.4 | 2.620 |
-2 | 2 | 4 | 2 | 34.259 | 0.5 | 2.615 |
2 | -2 | 4 | 2 | 34.259 | 0.5 | 2.615 |
3 | 3 | 1 | 2 | 34.282 | 0.5 | 2.614 |
-4 | -1 | 1 | 2 | 34.447 | 0.3 | 2.601 |
-1 | -4 | 1 | 2 | 34.447 | 0.3 | 2.601 |
1 | 4 | 0 | 2 | 34.525 | 0.1 | 2.596 |
4 | 1 | 0 | 2 | 34.525 | 0.2 | 2.596 |
-2 | 0 | 6 | 2 | 34.552 | 0.2 | 2.594 |
0 | -2 | 6 | 2 | 34.552 | 0.1 | 2.594 |
2 | -3 | 0 | 2 | 34.630 | 0.1 | 2.588 |
3 | -2 | 0 | 2 | 34.630 | 0.1 | 2.588 |
0 | 3 | 4 | 2 | 34.664 | 0.0 | 2.586 |
3 | 0 | 4 | 2 | 34.664 | 0.1 | 2.586 |
1 | 3 | 4 | 2 | 34.781 | 0.0 | 2.577 |
3 | 1 | 4 | 2 | 34.781 | 0.1 | 2.577 |
-3 | 2 | 1 | 2 | 34.931 | 0.1 | 2.567 |
2 | -3 | 1 | 2 | 34.931 | 0.1 | 2.567 |
-3 | -1 | 5 | 2 | 34.938 | 0.1 | 2.566 |
-1 | -3 | 5 | 2 | 34.938 | 0.1 | 2.566 |
-2 | 3 | 1 | 2 | 35.119 | 0.2 | 2.553 |
3 | -2 | 1 | 2 | 35.119 | 0.2 | 2.553 |
-4 | -1 | 2 | 2 | 35.161 | 0.2 | 2.550 |
-1 | -4 | 2 | 2 | 35.161 | 0.2 | 2.550 |
-3 | -3 | 3 | 2 | 35.179 | 0.2 | 2.549 |
0 | 4 | 0 | 2 | 35.255 | 0.1 | 2.544 |
4 | 0 | 0 | 2 | 35.255 | 0.1 | 2.544 |
-4 | 0 | 1 | 2 | 35.273 | 0.1 | 2.542 |
0 | -4 | 1 | 2 | 35.273 | 0.1 | 2.542 |
-3 | 1 | 4 | 2 | 35.334 | 0.0 | 2.538 |
1 | -3 | 4 | 2 | 35.334 | 0.0 | 2.538 |
1 | 4 | 1 | 2 | 35.389 | 0.0 | 2.534 |
4 | 11 | 2 | 2 | 35.389 | 0.0 | 2.534 |
No data available
No 3D representation available
No data available
No data available