Synthesis
Mixture | 1.0 SiO2 : 0.8 SDA : 0.05 Al(OH)3 : 26.3 H2O : 0.025 LiOH |
SDA | Ethyltrimethylammonium |
Temperature | 100.00 °C |
Duration | 150 d |
Conditions | n/a |
Reference |
Miller, Miller, Broach, Galey, Prabhakar, Lyons, Nicholas & Nicholas (2015): Microporous and Mesoporous Materials, Volume 202, Issue , Pages 250-258. |
Crystal Structure
Structurally nearly identical materials | None |
Crystal chemically related materials | None |
Chemical composition per unit cell | [N(CH3)3C2H5]8[H8Si24O56] ∙ 20 H2O |
Lattice parameters of the 2D cell of the layer |
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Lattice parameters related to the stacking direction |
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Space group | Ibam |
XRD reflections representing the 2D cell of the layer |
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XRD reflections representing the layer-layer distance |
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Reference |
Miller, Miller, Broach, Galey, Prabhakar, Lyons, Nicholas & Nicholas (2015): Microporous and Mesoporous Materials, Volume 202, Issue , Pages 250-258. |
Properties
Density (calculated) | 1.537 g/cm3 |
Condensation product | amorphous |
h | k | l | M | 2θ | Icalc | d-hkl |
---|---|---|---|---|---|---|
2 | 0 | 0 | 2 | 6.110 | 100.0 | 14.455 |
1 | 1 | 0 | 4 | 10.984 | 0.8 | 8.049 |
4 | 0 | 0 | 2 | 12.237 | 0.1 | 7.227 |
3 | 1 | 0 | 4 | 13.994 | 0.0 | 6.323 |
2 | 1 | 1 | 8 | 14.407 | 1.3 | 6.143 |
0 | 0 | 2 | 2 | 15.305 | 1.7 | 5.785 |
2 | 0 | 2 | 4 | 16.493 | 8.5 | 5.370 |
4 | 1 | 1 | 8 | 17.915 | 14.2 | 4.947 |
6 | 0 | 0 | 2 | 18.399 | 0.0 | 4.818 |
5 | 1 | 0 | 4 | 18.630 | 0.4 | 4.759 |
1 | 1 | 2 | 8 | 18.877 | 1.0 | 4.697 |
4 | 0 | 2 | 4 | 19.642 | 5.5 | 4.516 |
3 | 1 | 2 | 8 | 20.795 | 0.2 | 4.268 |
0 | 2 | 0 | 2 | 21.187 | 1.7 | 4.190 |
2 | 2 | 0 | 4 | 22.070 | 0.0 | 4.024 |
. | . | . | . | . | . | |
6 | 1 | 1 | 8 | 22.614 | 10.8 | 3.929 |
1 | 2 | 1 | 8 | 22.762 | 6.8 | 3.904 |
7 | 1 | 0 | 4 | 24.003 | 1.6 | 3.704 |
6 | 0 | 2 | 4 | 24.018 | 0.0 | 3.702 |
5 | 1 | 2 | 8 | 24.198 | 1.1 | 3.675 |
3 | 2 | 1 | 8 | 24.390 | 0.2 | 3.647 |
4 | 2 | 0 | 4 | 24.538 | 2.6 | 3.625 |
8 | 0 | 0 | 2 | 24.616 | 1.7 | 3.614 |
2 | 1 | 3 | 8 | 26.153 | 11.2 | 3.405 |
0 | 2 | 2 | 4 | 26.242 | 3.7 | 3.393 |
2 | 2 | 2 | 8 | 26.968 | 1.3 | 3.304 |
5 | 2 | 1 | 8 | 27.372 | 0.0 | 3.256 |
8 | 1 | 1 | 8 | 27.950 | 0.0 | 3.190 |
6 | 2 | 0 | 4 | 28.202 | 2.2 | 3.162 |
4 | 1 | 3 | 8 | 28.287 | 2.6 | 3.152 |
7 | 1 | 2 | 8 | 28.591 | 3.2 | 3.120 |
4 | 2 | 2 | 8 | 29.047 | 0.7 | 3.072 |
8 | 0 | 2 | 4 | 29.114 | 1.0 | 3.065 |
9 | 1 | 0 | 4 | 29.763 | 0.7 | 2.999 |
0 | 0 | 4 | 2 | 30.892 | 0.5 | 2.892 |
10 | 0 | 0 | 2 | 30.907 | 0.0 | 2.891 |
7 | 2 | 1 | 8 | 31.355 | 0.0 | 2.851 |
2 | 0 | 4 | 4 | 31.520 | 0.0 | 2.836 |
6 | 1 | 3 | 8 | 31.550 | 2.1 | 2.833 |
1 | 2 | 3 | 8 | 31.659 | 1.7 | 2.824 |
1 | 3 | 0 | 4 | 32.168 | 0.7 | 2.780 |
6 | 2 | 2 | 8 | 32.240 | 0.1 | 2.774 |
8 | 2 | 0 | 4 | 32.699 | 5.2 | 2.736 |
3 | 2 | 3 | 8 | 32.878 | 0.0 | 2.722 |
1 | 1 | 4 | 8 | 32.879 | 0.1 | 2.722 |
4 | 0 | 4 | 4 | 33.341 | 0.0 | 2.685 |
3 | 3 | 0 | 4 | 33.371 | 1.0 | 2.683 |
2 | 3 | 1 | 8 | 33.554 | 0.4 | 2.669 |
9 | 1 | 2 | 8 | 33.632 | 0.1 | 2.663 |
10 | 1 | 1 | 8 | 33.671 | 0.5 | 2.660 |
3 | 1 | 4 | 8 | 34.060 | 0.5 | 2.630 |
10 | 0 | 2 | 4 | 34.661 | 0.2 | 2.586 |
5 | 2 | 3 | 8 | 35.204 | 0.1 | 2.547 |
4 | 3 | 1 | 8 | 35.282 | 0.1 | 2.542 |
8 | 1 | 3 | 8 | 35.667 | 0.0 | 2.515 |
5 | 3 | 0 | 4 | 35.668 | 0.3 | 2.515 |
11 | 1 | 0 | 4 | 35.779 | 0.0 | 2.508 |
1 | 3 | 2 | 8 | 35.804 | 0.0 | 2.506 |
9 | 2 | 1 | 8 | 36.049 | 0.1 | 2.489 |
6 | 0 | 4 | 4 | 36.195 | 0.1 | 2.480 |
8 | 2 | 2 | 8 | 36.287 | 0.1 | 2.474 |
5 | 1 | 4 | 8 | 36.319 | 0.6 | 2.472 |
3 | 3 | 2 | 8 | 36.902 | 0.4 | 2.434 |
Atom | x | y | z | Biso | Occ. | |
---|---|---|---|---|---|---|
Si1 | 0.6912 | 0.2015 | 0.1351 | 3.36 | 1.000 | |
Si2 | 0.7329 | 0.5000 | 0.2500 | 3.36 | 1.000 | |
O1 | 0.6990 | 0.3789 | 0.1829 | 4.14 | 1.000 | |
O2 | 0.7390 | 0.0947 | 0.1563 | 4.14 | 1.000 | |
O3 | 0.6476 | 0.1334 | 0.1956 | 4.14 | 1.000 | |
O4 | 0.6830 | 0.2205 | 0.0000 | 4.14 | 1.000 | |
O5 | 0.0000 | 0.5000 | 0.2500 | 1.11 | 0.816 | |
O6 | 0.0589 | 0.2865 | 0.1240 | 4.03 | 0.873 | |
N1 | 0.1170 | 0.8173 | 0.0000 | 8.69 | 1.000 | |
C1 | 0.0791 | 0.6972 | 0.0000 | 8.69 | 1.000 | |
C2 | 0.6665 | 0.7344 | 0.0000 | 8.69 | 1.000 | |
C3 | 0.1015 | -0.0920 | 0.1045 | 8.69 | 1.000 | |
C4 | 0.0491 | 0.9490 | 0.1086 | 8.69 | 0.500 |
User Cell Range (natural numbers 1-5):
No data available